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[ CAS No. 1433029-60-7 ] {[proInfo.proName]}

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Chemical Structure| 1433029-60-7
Chemical Structure| 1433029-60-7
Structure of 1433029-60-7 * Storage: {[proInfo.prStorage]}
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Product Details of [ 1433029-60-7 ]

CAS No. :1433029-60-7 MDL No. :N/A
Formula : C21H13NO8 Boiling Point : -
Linear Structure Formula :- InChI Key :WDFYUCKWERMMKR-UHFFFAOYSA-N
M.W : 407.33 Pubchem ID :102206396
Synonyms :

Safety of [ 1433029-60-7 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P264-P271-P280-P302+P352-P304+P340+P312-P305+P351+P338-P332+P313-P337+P313-P362-P403+P233-P405-P501 UN#:N/A
Hazard Statements:H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 1433029-60-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1433029-60-7 ]

[ 1433029-60-7 ] Synthesis Path-Downstream   1~10

  • 1
  • [ 1433029-53-8 ]
  • [ 1433029-60-7 ]
YieldReaction ConditionsOperation in experiment
With water; sodium hydroxide In tetrahydrofuran; methanol at 20℃;
  • 2
  • [ 625-92-3 ]
  • [ 1309982-02-2 ]
  • [ 1433029-60-7 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: cesium fluoride; tetrakis(triphenylphosphine) palladium(0) / 1,2-dimethoxyethane / 72 h / Schlenk technique; Inert atmosphere; Reflux 2: sodium hydroxide; water / tetrahydrofuran; methanol / 20 °C
  • 3
  • [ 288-94-8 ]
  • zinc(II) nitrate hexahydrate [ No CAS ]
  • [ 1433029-60-7 ]
  • [ 33513-42-7 ]
  • [Me2NH2][Zn2(3,5-bis(3,5-dicarboxylphenyl)pyridine)(1H-tetrazole)]·4DMF [ No CAS ]
YieldReaction ConditionsOperation in experiment
54% With nitric acid at 105℃; for 72h;
  • 4
  • [ 4418-61-5 ]
  • zinc(II) nitrate hexahydrate [ No CAS ]
  • [ 1433029-60-7 ]
  • [ 33513-42-7 ]
  • [Me2NH2][Zn2(3,5-bis(3,5-dicarboxylphenyl)pyridine)(5-amino-1H-tetrazole)]·4DMF [ No CAS ]
YieldReaction ConditionsOperation in experiment
49% With nitric acid at 105℃; for 72h;
  • 5
  • terbium(III) nitrate hexahydrate [ No CAS ]
  • [ 1433029-60-7 ]
  • [ 7732-18-5 ]
  • [ 33513-42-7 ]
  • [(CH3)2NH2]2[Tb2(5,5′-(pyridine-3,5-diyl)-diisophthalate)2(H2O)2]·2N,N-dimethylformamide·2H2O [ No CAS ]
YieldReaction ConditionsOperation in experiment
0.62% With nitric acid at 160℃; for 72h; High pressure;
  • 6
  • europium(III) nitrate hexahydrate [ No CAS ]
  • [ 1433029-60-7 ]
  • [ 7732-18-5 ]
  • [ 33513-42-7 ]
  • [(CH3)2NH2]2[Eu2(5,5′-(pyridine-3,5-diyl)-diisophthalate)2(H2O)2]·2N,N-dimethylformamide·2H2O [ No CAS ]
YieldReaction ConditionsOperation in experiment
0.62% With nitric acid at 160℃; for 72h; High pressure;
  • 7
  • gadolinium(III) nitrate hexahydrate [ No CAS ]
  • [ 1433029-60-7 ]
  • [ 7732-18-5 ]
  • [ 33513-42-7 ]
  • [(CH3)2NH2]2[Gd2(5,5′-(pyridine-3,5-diyl)-diisophthalate)2(H2O)2]·2N,N-dimethylformamide·2H2O [ No CAS ]
YieldReaction ConditionsOperation in experiment
0.68% With nitric acid at 160℃; for 72h; High pressure;
  • 8
  • europium(III) nitrate hexahydrate [ No CAS ]
  • [ 1433029-60-7 ]
  • [ 33513-42-7 ]
  • C21H9NO8(4-)*Eu(3+)*H(1+)*C2H7N*2H2O [ No CAS ]
YieldReaction ConditionsOperation in experiment
83% With sodium hydroxide In water at 120℃; for 72h; Autoclave; High pressure; 2.2 Synthesis of {(Me2NH2+)[Ln(L)(H2O)2]n (1-5) [Ln=Eu(1), Tb(2), Gd(3), Sm(4) and Pr(5)] All compounds were obtained by adopting an identical procedure except for the different starting lanthanide salts. The synthesis of {(Me2NH2+)[Eu(L)(H2O) is thus presented here in detail as a representative: a mixture of Eu(NO3)3·6H2O (44.6mg, 0.1mmol), H4L (0.0203g, 0.05mmol), distilled water (2.5mL), DMF (2.5mL) (DMF=N,N’-dimethylformamide) and NaOH (1M, 20µL) was sealed in a 25mL Teflon-lined autoclave and then heated at 120°C for 72h. After cooling to room temperature, block crystals were obtained. Yield: 83% for 1, 82% for 2, 85% for 3, 68% for 4 and 62% for 5 (based on the H4L ligand). Elemental analysis (%) for 1 (637.38), calcd: C, 43.34; H, 3.32; N, 4.40. Found: C, 43.36; H, 3.26; N, 4.51%. IR (KBr, cm-1): 3415(m), 1614(s) , 1554(s), 1439(w), 1401(w), 1361(m), 899(w), 779(s), 730(s), 656(m). Elemental analysis (%) for 2 (644.35), calcd: C, 42.87; H, 3.29; N, 4.35. Found: C, 43.08; H, 3.02; N, 4.31%. IR (KBr, cm-1): 3419(m), 1613(s) , 1550(s), 1435(w), 1395(w), 1361(m), 883(w), 779(s), 725(s), 656(w). Elemental analysis (%) for 3 (642.67), calcd: C, 42.98; H, 3.29; N, 4.36. Found: C, 43.10; H, 3.08; N, 4.30%. IR (KBr, cm-1): 3425(m), 1619(s), 1552(s), 1435(w), 1398(w), 1362(s), 1301(w), 1251(w), 1018(w), 899(w), 778(s), 729(s), 656(m). Elemental analysis (%) for 4 (635.78), calcd: C, 43.45; H, 3.33; N, 4.41. Found: C, 43.50; H, 3.42; N, 4.41%. IR (KBr, cm-1): 3425(m), 1619(s), 1564(s), 1435(w), 1400(w), 1370(m), 889(w), 778(s), 719(s), 656(m). Elemental analysis (%) for 5 (626.33), calcd: C, 44.11; H, 3.38; N, 4.47. Found: C, 43.23; H, 3.41; N, 4.41%. IR (KBr, cm-1): 3424(m), 1614(s), 1556(s), 1443(w), 1405(w), 1367(m), 893(w), 775(s), 738(s), 657(m).
  • 9
  • [ 288-32-4 ]
  • copper(II) nitrate trihydrate [ No CAS ]
  • [ 1433029-60-7 ]
  • [ 33513-42-7 ]
  • [Me2NH2][Cu2(BDPP)(im)]*3DMF}n [ No CAS ]
YieldReaction ConditionsOperation in experiment
68% With nitric acid In water at 105℃; for 72h; High pressure; 2.2. Preparation and characterization for [Me2NH2][Cu2(BDPP)(im)]3DMF}n (1) We put Cu(NO3)23H2O which is 0.1mmol and 0.024g, H4BDPP of 0.04mmol and 0.016g as well as Him which is 0.2mmol and 0.012g, mixed them to form a mixture, and the mixture was dissolved in H2O of 1mL and DMF 6mL. After the addition of HNO3 (1mL, 2M) in a 10mL screw-capped vial at room temperature, the reaction mixture was placed for 3days at 105°C in an oven. By isolating we obtained blue diamond crystals of 1 (with a yield of 68% on the basis of H4BDPP). Anal. Calcd. (%) for C35H41Cu2N7O11 (1): C, 48.72; H, 4.79; N, 11.36. Found: C, 48.38; H, 4.64; N, 4.068.
  • 10
  • europium(III) chloride hexahydrate [ No CAS ]
  • [ 1433029-60-7 ]
  • [ 7732-18-5 ]
  • [ 33513-42-7 ]
  • 2C21H9NO8(4-)*2Eu(3+)*4H2O*2H(1+)*2C3H7NO*2.5C3H4N2 [ No CAS ]
YieldReaction ConditionsOperation in experiment
46% In acetic acid at 160℃; for 72h;
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