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[ CAS No. 138479-54-6 ] {[proInfo.proName]}

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Chemical Structure| 138479-54-6
Chemical Structure| 138479-54-6
Structure of 138479-54-6 * Storage: {[proInfo.prStorage]}
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Product Details of [ 138479-54-6 ]

CAS No. :138479-54-6 MDL No. :MFCD11156565
Formula : C9H7N3O2 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 189.17 Pubchem ID :-
Synonyms :

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Application In Synthesis of [ 138479-54-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 138479-54-6 ]

[ 138479-54-6 ] Synthesis Path-Downstream   1~11

  • 1
  • [ 288-88-0 ]
  • [ 446-52-6 ]
  • [ 138479-54-6 ]
YieldReaction ConditionsOperation in experiment
53% With potassium carbonate In dimethyl sulfoxide at 100℃; for 10h;
  • 2
  • [ 138479-53-5 ]
  • [ 138479-54-6 ]
YieldReaction ConditionsOperation in experiment
With potassium hydroxide; potassium permanganate at 100℃;
  • 5
  • [ 138479-54-6 ]
  • [ 137973-03-6 ]
  • [ 730927-66-9 ]
YieldReaction ConditionsOperation in experiment
Stage #1: 2-(1',2',4'-triazol-1'-yl)benzoic acid With 4-methyl-morpholine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane for 1h; cooling; Stage #2: 6-<(4-aminophenyl)carbonyl>-2,6-diazabicyclo<5.4.0>undeca-1(7),8,10-trien-3-one In dichloromethane at 20℃;
  • 6
  • [ 394-47-8 ]
  • [ 138479-54-6 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: K2CO3 / dimethylsulfoxide / 3 h / 100 °C 2: aq. KOH / 2-ethoxy-ethanol / 3 h / Heating
Multi-step reaction with 2 steps 1: 69 percent / K2CO3 / dimethylsulfoxide / 3 h / 100 °C 2: 81 percent / acetic acid, conc. H2SO4, H2O / 5 h / Heating
Multi-step reaction with 3 steps 1.1: potassium carbonate / N,N-dimethyl-formamide / 85 °C 2.1: sulfuric acid; water / Reflux 3.1: sulfuric acid; sodium nitrite / 0 - 10 °C 3.2: 2 h / 100 °C
  • 7
  • [ 446-52-6 ]
  • [ 138479-54-6 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: 24 percent / K2CO3 / dimethylsulfoxide / 3 h / 100 °C 2: 61 percent / 5 M aq. KOH / ethanol / 1 h / Heating
YieldReaction ConditionsOperation in experiment
With sulfuric acid; water; sodium nitrite at 0 - 100℃; for 3h; 24 Step 3 General procedure: Add 14.3 g (0.064 mol) of 2-chloro-6-(1H-1, 2,4-triazol-1-yl)benzamide to a 100 mL three-necked reaction flask, and place the three-necked flask in an ice bath In the range of 0 10 ,Slowly add 79 g of 80% sulfuric acid (0.64 mol) aqueous solution, and after dropping, start to add dropwise an aqueous solution made of 22.1 g (0.32 mol) sodium nitrite that has been cooled to 0 10 ,Keep the reaction always between 0 ~ 10 , after the dropwise addition, keep the reaction for 1h. Then react at 100 for 2h,TLC detected the completion of the reaction. The reaction solution was extracted with ethyl acetate, dried, and the solvent was distilled off under reduced pressure to obtain a pale yellow solid of 2-chloro-6-(1H-1,2,4-triazol-1-yl)benzoic acid 12 g.2-chloro-6-(1H-1,2,4-triazol-1-yl)benzoic acid, yellow solid,. Yield: 84%.
  • 9
  • [ 138479-54-6 ]
  • [ 2459310-24-6 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: thionyl chloride / 80 °C 2: triethylamine / 80 - 100 °C
  • 11
  • [ 1340348-27-7 ]
  • [ 138479-54-6 ]
YieldReaction ConditionsOperation in experiment
Stage #1: (1,2,4-triazol-1-yl)benzamide With sulfuric acid; sodium nitrite at 0 - 10℃; Stage #2: With sulfuric acid; water at 100℃;
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