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CAS No. : | 1044589-82-3 | MDL No. : | MFCD27952796 |
Formula : | C13H14N4O4 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 290.27 | Pubchem ID : | - |
Synonyms : |
7-Deaza-2'-C-acetylene-adenosine
|
Signal Word: | Class: | N/A | |
Precautionary Statements: | UN#: | N/A | |
Hazard Statements: | Packing Group: | N/A |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 6 steps 1.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; trichloroisocyanuric acid / dichloromethane / 20 °C / Cooling with ice 2.1: tetrahydrofuran / 3 h / 0 °C 2.2: Cooling 3.1: hydrogen bromide; acetic acid / dichloromethane / 1.5 h / 20 °C 4.1: sodium hydride / acetonitrile / 0.5 h / 20 °C 4.2: 18 h / 20 °C 5.1: boron trichloride / dichloromethane / -78 °C 5.2: 0.5 h / 0 °C 6.1: ammonia / water / 5 h / 100 °C |