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[ CAS No. 914348-93-9 ] {[proInfo.proName]}

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Chemical Structure| 914348-93-9
Chemical Structure| 914348-93-9
Structure of 914348-93-9 * Storage: {[proInfo.prStorage]}
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Product Details of [ 914348-93-9 ]

CAS No. :914348-93-9 MDL No. :MFCD05864692
Formula : C15H14N2O3 Boiling Point : -
Linear Structure Formula :- InChI Key :MLUMALLEGSYCHN-UHFFFAOYSA-N
M.W : 270.28 Pubchem ID :40428519
Synonyms :

Safety of [ 914348-93-9 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P280-P305+P351+P338 UN#:N/A
Hazard Statements:H302-H315-H319-H332-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 914348-93-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Upstream synthesis route of [ 914348-93-9 ]
  • Downstream synthetic route of [ 914348-93-9 ]

[ 914348-93-9 ] Synthesis Path-Upstream   1~1

  • 1
  • [ 24424-99-5 ]
  • [ 17380-18-6 ]
  • [ 914348-93-9 ]
YieldReaction ConditionsOperation in experiment
0.379 g With dmap In acetonitrile at 20℃; General procedure: To a solution of an appropriate indole, azaindole or alternative heterocycles (1.0 eq) and di-ferf-butyl dicarbonate (1eq. to 2 eq., more in particular 1.2 eq) in acetonitrile was added DMAP (0.1 to 0.5 eq. more in particular 0.1 eq). The reaction mixture was stirred overnight at room temperature. The reaction mixture was concentrated under reduced pressure. The residue was dissolved in dichloromethane and washed with a saturated sodium bicarbonate solution. The phases were separated. The aqueous phase was extracted with dichloromethane. The organic phases were combined, washed with a saturated ammonium chloride solution, water and brine, dried over magnesium sulfate, filtered and concentrated under reduced pressure. The BOC-protected compound was used in the next step without further purification.
Reference: [1] Patent: WO2013/45516, 2013, A1, . Location in patent: Page/Page column 129; 179
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