Alternatived Products of [ 82452-98-0 ]
Product Details of [ 82452-98-0 ]
CAS No. : | 82452-98-0 |
MDL No. : | MFCD22565716 |
Formula : |
C8H5IN2O
|
Boiling Point : |
- |
Linear Structure Formula : | - |
InChI Key : | - |
M.W : |
272.04
|
Pubchem ID : | - |
Synonyms : |
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Safety of [ 82452-98-0 ]
Signal Word: | |
Class: | |
Precautionary Statements: | |
UN#: | |
Hazard Statements: | |
Packing Group: | |
Application In Synthesis of [ 82452-98-0 ]
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
- Downstream synthetic route of [ 82452-98-0 ]
- 1
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[ 18514-84-6 ]
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[ 82452-98-0 ]
- 2
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[ 78593-40-5 ]
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[ 82452-98-0 ]
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[ 82453-23-4 ]
- 3
-
[ 78593-42-7 ]
-
[ 82452-98-0 ]
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[ 82453-24-5 ]
- 4
-
[ 19419-09-1 ]
-
[ 82452-98-0 ]
Yield | Reaction Conditions | Operation in experiment |
80% |
With N-iodo-succinimide In N,N-dimethyl-formamide at 60℃; for 3h; |
3
Intermediate 3: Preparation of 3-Iodo-l,4-dihydro-4-cinnolinone:A solution of cinnolinone and N-iodosuccinimide in DMF was stirred at 60°C for 3h. The mixture was poured into water and the precipitated product was collected by filtration and dried under vacuum. Appearance: Off-white powder. Yield: 80%. 1H-NMR (δ ppm, CDCl3, 300 MHz): 13.90 (br. s, IH); 8.02 (d, J = 7.8, IH); 7.82 (t, J = 6.9, IH); 7.58 (d, J = 8.1, IH); 7.48 (t, J = 7.5, IH). |