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[ CAS No. 82452-98-0 ] {[proInfo.proName]}

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Chemical Structure| 82452-98-0
Chemical Structure| 82452-98-0
Structure of 82452-98-0 * Storage: {[proInfo.prStorage]}
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Product Details of [ 82452-98-0 ]

CAS No. :82452-98-0 MDL No. :MFCD22565716
Formula : C8H5IN2O Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 272.04 Pubchem ID :-
Synonyms :

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Application In Synthesis of [ 82452-98-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 82452-98-0 ]

[ 82452-98-0 ] Synthesis Path-Downstream   1~4

  • 1
  • [ 18514-84-6 ]
  • [ 82452-98-0 ]
  • 2
  • [ 78593-40-5 ]
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  • [ 82453-23-4 ]
  • 3
  • [ 78593-42-7 ]
  • [ 82452-98-0 ]
  • [ 82453-24-5 ]
  • 4
  • [ 19419-09-1 ]
  • [ 82452-98-0 ]
YieldReaction ConditionsOperation in experiment
80% With N-iodo-succinimide In N,N-dimethyl-formamide at 60℃; for 3h; 3 Intermediate 3: Preparation of 3-Iodo-l,4-dihydro-4-cinnolinone:A solution of cinnolinone and N-iodosuccinimide in DMF was stirred at 60°C for 3h. The mixture was poured into water and the precipitated product was collected by filtration and dried under vacuum. Appearance: Off-white powder. Yield: 80%. 1H-NMR (δ ppm, CDCl3, 300 MHz): 13.90 (br. s, IH); 8.02 (d, J = 7.8, IH); 7.82 (t, J = 6.9, IH); 7.58 (d, J = 8.1, IH); 7.48 (t, J = 7.5, IH).
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