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[ CAS No. 655254-61-8 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
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Type HazMat fee for 500 gram (Estimated)
Excepted Quantity USD 0.00
Limited Quantity USD 15-60
Inaccessible (Haz class 6.1), Domestic USD 80+
Inaccessible (Haz class 6.1), International USD 150+
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Chemical Structure| 655254-61-8
Chemical Structure| 655254-61-8
Structure of 655254-61-8 * Storage: {[proInfo.prStorage]}
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Product Details of [ 655254-61-8 ]

CAS No. :655254-61-8 MDL No. :MFCD04114782
Formula : C15H12BrNO2S Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 350.23 Pubchem ID :-
Synonyms :

Safety of [ 655254-61-8 ]

Signal Word:Danger Class:6.1
Precautionary Statements:P260-P262-P264-P270-P271-P280-P284-P301+P310+P330-P302+P352+P310-P304+P340+P310-P361+P364-P403+P233-P405-P501 UN#:2811
Hazard Statements:H300+H310+H330 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 655254-61-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 655254-61-8 ]

[ 655254-61-8 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 728034-12-6 ]
  • [ 655254-61-8 ]
  • [ 108-91-8 ]
  • 4-(4-(4-bromophenyl)-1-cyclohexyl-1H-imidazol-5-yl)-1H-pyrrolo[2,3-b]pyridine [ No CAS ]
YieldReaction ConditionsOperation in experiment
11% General procedure: To a solutionof the corresponding aldehyde (1.2 eq.; unless stated otherwise) in DMF (2 inL per 0.3 mmol of aldehyde; unless stated otherwise) was added the corresponding amine (2.5 eq.; unless stated otherwise) and the resulting solution was stirred at 25 C to form the corresponding inline. Then, the corresponding isocyano(tosyl)methyl)arene reagent (1 eq.; unless stated otherwise) and K2CO3 (1.5 eq.; unless stated otherwise*) were added and the reaction mixture was stirred at 25 C (unless stated otherwise). The reaction was stopped after the time indicated for each particular reaction. The reaction progress was monitored by TLC. (0083) A saturated aqueous solution of NH4CI (10 mL per 1 mmol of aldehyde) was added to the reaction mixture, which was then extracted with EtOAc (2 x 30 mL per 1 mmol of aldehyde). The combined organic extracts were washed with H2O (2 x 25 mL per 1 mmol of aldehyde), dried over MgSCC, filtered, and the solvent was evaporated in vacuo to provide the crude product. The residue obtained after the workup was purified using column chromatography or preparative TLC (unless stated otherwise). (0084) * note: in cases when the amine was used as HC1 salt, 4 eq. of K2CO3 were used
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