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[ CAS No. 6470-87-7 ] {[proInfo.proName]}

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Chemical Structure| 6470-87-7
Chemical Structure| 6470-87-7
Structure of 6470-87-7 * Storage: {[proInfo.prStorage]}
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Product Details of [ 6470-87-7 ]

CAS No. :6470-87-7 MDL No. :MFCD00059498
Formula : C15H7ClO3 Boiling Point : -
Linear Structure Formula :- InChI Key :DGJNWQJOASAMHY-UHFFFAOYSA-N
M.W : 270.67 Pubchem ID :15025286
Synonyms :

Safety of [ 6470-87-7 ]

Signal Word:Danger Class:8
Precautionary Statements:P234-P260-P264-P280-P301+P330+P331+P310-P303+P361+P353+P310+P363-P304+P340+P310-P305+P351+P338+P310-P390-P405-P406-P501 UN#:3261
Hazard Statements:H290-H314 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 6470-87-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 6470-87-7 ]

[ 6470-87-7 ] Synthesis Path-Downstream   1~7

  • 1
  • [ 117-78-2 ]
  • [ 6470-87-7 ]
YieldReaction ConditionsOperation in experiment
With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; for 2h;Inert atmosphere; This example and the following Examples 2 and 3 describe compounds and methods of the invention for making an ASM-amide-linked sol-gel matrix material and corresponding WE of the invention. Anthraquinone-2-carboxylic acid (0.500 g, 1.98 mmol) was suspended in dichloromethane (20 mL) in a vial, and then the vial was purged with nitrogen. 0.2 mL of dimethylformamide (DMF) was added dropwise, followed by addition of oxalyl chloride (0.18 mL, 2.2 mmol). The solution was stirred for 2 h. Then, diethylaminomethylpolystyrene (1.97 g, 6.3 mmol of amine) was added followed by 3-aminopropyltrimethoxysilane (APTOS) (0.37 mL, 2.1 mmol). Stirring was continued for 16 h at ambient temperature. The resultant liquid was filtered to remove the diethylaminomethylpolystyrene solid. Additional dichloromethane was used to rinse the retained solid to recover entrained product. The dichloromethane was removed in a rotary evaporator to obtain an amber oily liquid. Anhydrous alcohol was used to reconstitute the oily liquid to obtain 20 mL of the amide-linked AQ silane solution.
With thionyl chloride; N,N-dimethyl-formamide; In dichloromethane;Reflux; 9,10-<strong>[117-78-2]anthraquinone-2-carboxylic acid</strong> (1.86 g, 7.4 mmol) was added to a 100 mL reaction flask,Thionyl chloride (1.05 g, 8.9 mmol), dichloromethane (30 mL), catalytic amount of DMF, reflux reaction overnight, to be completely clear solution to be -9,10-anthraquinone-2-formyl chloride in dichloromethane solution, Directly for the next step
Reference: [1]European Journal of Medicinal Chemistry,2007,vol. 42,p. 752 - 771
[2]Journal of Organic Chemistry,1992,vol. 57,p. 6143 - 6150
[3]Chemistry - A European Journal,2002,vol. 8,p. 5630 - 5643
[4]Journal of the American Chemical Society,1994,vol. 116,p. 9847 - 9859
[5]Journal of the Indian Chemical Society,1932,vol. 9,p. 375
[6]Bulletin of the Chemical Society of Japan,1932,vol. 7,p. 114,117, 118
[7]Chemische Berichte,1884,vol. 17,p. 890
[8]Helvetica Chimica Acta,1926,vol. 9,p. 802
[9]Liebigs Annalen der Chemie,1981,p. 792 - 810
[10]Journal of Medicinal Chemistry,1982,vol. 25,p. 369 - 373
[11]Journal of the American Chemical Society,1989,vol. 111,p. 5542 - 5551
[12]Helvetica Chimica Acta,1980,vol. 63,p. 413 - 419
[13]Journal of Organic Chemistry,1996,vol. 61,p. 1297 - 1301
[14]Journal of Physical Chemistry A,2000,vol. 104,p. 8315 - 8322
[15]Bulletin of the Chemical Society of Japan,2000,vol. 73,p. 2051 - 2058
[16]Organic letters,2000,vol. 2,p. 3413 - 3416
[17]Journal of Organic Chemistry,2000,vol. 65,p. 5355 - 5359
[18]Chemical Communications,2009,p. 5281 - 5283
[19]European Journal of Inorganic Chemistry,2014,vol. 2014,p. 1984 - 2001
[20]Patent: US9417204,2016,B2 .Location in patent: Page/Page column 24; 25
[21]Patent: CN104788333,2017,B .Location in patent: Paragraph 0189-0191
[22]Chemical Biology and Drug Design,2018,vol. 91,p. 893 - 901
[23]Chemical Communications,2018,vol. 54,p. 3038 - 3041
[24]Angewandte Chemie - International Edition,2018,vol. 57,p. 16871 - 16876
    Angew. Chem.,2018,vol. 130,p. 17113 - 17118,6
  • 2
  • [ 1454-85-9 ]
  • [ 6470-87-7 ]
  • [ 143657-42-5 ]
  • 3
  • [ 144183-31-3 ]
  • [ 6470-87-7 ]
  • [ 144183-33-5 ]
YieldReaction ConditionsOperation in experiment
41% With triethylamine In dichloromethane
  • 4
  • [ 15430-52-1 ]
  • [ 6470-87-7 ]
  • [ 309924-33-2 ]
  • 5
  • [ 17812-32-7 ]
  • [ 6470-87-7 ]
  • C20H15NO7 [ No CAS ]
  • 6
  • [ 6384-08-3 ]
  • [ 6470-87-7 ]
  • C21H17NO7 [ No CAS ]
  • 7
  • [ 6384-08-3 ]
  • [ 6470-87-7 ]
  • N-(9,10-anthraquinone-2-formyl)-L-glutamic acid [ No CAS ]
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