Alternatived Products of [ 38560-28-0 ]
Product Details of [ 38560-28-0 ]
CAS No. : | 38560-28-0 |
MDL No. : | MFCD22690543 |
Formula : |
C9H8BrNO
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Boiling Point : |
- |
Linear Structure Formula : | - |
InChI Key : | - |
M.W : |
226.07
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Pubchem ID : | - |
Synonyms : |
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Application In Synthesis of [ 38560-28-0 ]
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
- Downstream synthetic route of [ 38560-28-0 ]
- 1
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[ 38560-28-0 ]
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[ 114417-34-4 ]
Yield | Reaction Conditions | Operation in experiment |
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Stage #1: 1-(3-bromo-phenyl)-azetidin-2-one With trifluorormethanesulfonic acid In 1,2-dichloro-ethane at 20℃; for 1h;
Stage #2: With sodium hydrogencarbonate In water; 1,2-dichloro-ethane |
102C
Example 102C; 5.0 g (33 mMol) of trifluoromethanesulfonic acid [CAS No. 1493-13-6] was added to a solution of 28 mMol of the compound from example 102B in 250 mls of dichloroethane and the solution was stirred for 1 hour at ambient temperature. The reaction was washed with 10% NaHCO3, water, and saturated NaCl the organic layer was dried with MgSO4, filtered and the solvent evaporated. The resulting oil was further purified by flash chromatography using a gradient from hexane to 40% ethyl acetate in hexane then 100% ethyl acetate to provide Example 102C. |