[ CAS No. 351498-10-7 ] {[proInfo.proName]}

Name: 351498-10-7|6,6'-((1E,1'E)-((2,3-Dimethylbutane-2,3-diyl)bis(azanylylidene))bis(methanylylidene))bis(2,4-di-tert-butylphenol)|98%
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Quality Control of [ 351498-10-7 ]

COA NMR CNMR HPLC LC-MS

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SDS Specification

Alternatived Products of [ 351498-10-7 ]

Product Details of [ 351498-10-7 ]

CAS No. :	351498-10-7	MDL No. :	MFCD06797077
Formula :	C₃₆H₅₆N₂O₂	Boiling Point :	-
Linear Structure Formula :	-	InChI Key :	ZTDNTQMYPZYXNP-UHFFFAOYSA-N
M.W :	548.84	Pubchem ID :	135404188
Synonyms :

Safety of [ 351498-10-7 ]

Signal Word:	Warning	Class:	N/A
Precautionary Statements:	P261-P305+P351+P338	UN#:	N/A
Hazard Statements:	H302-H315-H319-H335	Packing Group:	N/A
GHS Pictogram:

Application In Synthesis of [ 351498-10-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

Downstream synthetic route of [ 351498-10-7 ]

[ 351498-10-7 ] Synthesis Path-Downstream 1~9

1
[ 351498-10-7 ]
[ 7732-18-5 ]
[ 557-20-0 ]
1,1,2,2-tetramethyl-1,2-ethanediamino-N,N'-bis(3,5-di-tert-butylsalicylidene) zinc(II)*1/4H₂O [ No CAS ]

Reference： [1]Inorganic Chemistry,2001,vol. 40,p. 3222 - 3227

2
[ 351498-10-7 ]
[ 6147-53-1 ]
[ 157472-96-3 ]

Reference： [1]Acta Crystallographica, Section C: Crystal Structure Communications,1998,vol. 54,p. 20 - 22

3
[ 351498-10-7 ]
[ 157472-96-3 ]

Yield	Reaction Conditions	Operation in experiment
75%	With cobalt(II) acetate; In ethanol; for 3.0h;Reflux;	Preparation of Cobalt(ll) Complex used in Step 2: A 50 mL flask was charged with lambda/,lambda/-bis(3,5-di-tert-butylsalicylidene)-1 , 1 ,2,2- tetramethylethenediamine (0.4302 g, 0.78 mmol, 1.0 equiv), EtOH (17 mL), and Co(OAc)2 (0.1385 g, 0.78 mmol, 1.0 equiv). The mixture was degassed and then heated to reflux under nitrogen for 3 h, cooled to room temperature. The precipitate was filtered and the purple solid was washed with EtOH (10 mL) and dried under high vacuum to give 0.3533 g (75%) of the cobalt(ll) complex.

Reference： [1]Patent: WO2009/88997,2009,A1 .Location in patent: Page/Page column 100

4
[ 351498-10-7 ]
[ 71-48-7 ]
[ 157472-96-3 ]

Yield	Reaction Conditions	Operation in experiment
75%	In ethanol; for 3.0h;Heating / reflux;	Cobalt catalyst 1 was prepared as follows: A 50 mL flask was charged with lambda/,/V'-bis(3,5-di-fert-butylsalicylidene)-1 ,1 ,2,2-tetramethylethenediamine (0.4302 g, 0.78 mmol, 1.0 equiv), EtOH (17 mL), and Co(OAc)2 (0.1385 g, 0.78 mmol, 1.0 equiv). The mixture was degassed and then heated to reflux under nitrogen for 3 h, cooled to room temperature. The precipitate was filtered and the purple solid was washed with EtOH (10 mL) and dried under high vacuum to give 0.3533 g (75%) of the cobalt(l I) complex. <n="104"/>LC-MS Method 2 tR = 1.921 min, m/z = 440.1 ; 1H NMR (CD3OD) delta=1.25 (s, 3H), 1.49 (s, 3H), 2.04 (d, 3H), 2.34 (m, 2H), 2.38 (m, 1 H), 2.40 (m, 2H), 3.02 (m, 1H), 5.67 (m, 1 H), 6.97 (m, 2H), 7.26 (m, 3H), 7.38 (m, 4H).
75%	In ethanol; for 3.0h;Reflux; Inert atmosphere;	Preparation of Cobalt(II) ComplexA 50 mL flask was charged with N,N'-bis(3,5-di-tert-butylsalicylidene)-l, 1,2,2- tetramethylethenediamine (0.4302 g, 0.78 mmol, 1.0 equiv), EtOH (17 mL), and Co(OAc)2 (0.1385 g, 0.78 mmol, 1.0 equiv). The mixture was degassed and then heated to reflux under nitrogen for 3 h, cooled to room temperature. The precipitate was filtered and the purple solid was washed with EtOH (10 mL) and dried under high vacuum to give 0.3533 g (75%) of the cobalt(II) complex.
75%	In ethanol; for 3.0h;Inert atmosphere; Reflux;	A 50 mL flask was charged with N,N'-bis(3,5-di-tert-butylsalicylidene)-1,1,2,2-tetramethylethenediamine (0.430 g, 0.78 mmol, 1.0 equiv), EtOH (17 mL), and Co(OAc)2 (0.139 g, 0.78 mmol, 1.0 equiv). The mixture was degassed and then heated to reflux under nitrogen for 3 h, cooled to room temperature. The precipitate was filtered and the purple solid was washed with EtOH (10 mL) and dried under high vacuum to give 0.353 g (75%) of the cobalt(II) complex.

75%	In ethanol; for 3.0h;Reflux; Inert atmosphere;	A 50 ml. flask was charged withLambda/,Lambda/-bis(3,5-di-te/t-butylsalicylidene)-1 ,1 ,2,2-tetramethylethenediamine (0.4302 g, 0.78 mmol, 1.0 equiv), EtOH (17 ml_), and Co(OAc)2 (0.1385 g, 0.78 mmol, 1.0 equiv). The mixture was degassed and then heated to reflux under nitrogen for 3 h, cooled to room temperature. The precipitate was filtered and the purple solid was washed with EtOH (10 ml.) and dried under high vacuum to give 0.3533 g (75%) of the cobalt(ll) complex.
72%	In ethanol; at 80.0℃; for 2.0h;	EXAMPLE 1Preparation of Intermediate Compound Int-lclnt-1a n - c Compound Int-la (733 mg, 1.33 mmol) was suspended in ethanol (10 mL) and the resulting suspension was heated to 80 C and allowed to stir for 5 minutes. Compound Int- lb (236 mg, 1.33 mmol) was then added and the resulting reaction was allowed to stir at 80 C for an additional 2 hours. The reaction was then cooled to room temperature using in an ice bath and the reaction mixture was filtered. The collected red solid was dried under vacuum to provide compound Int-lc (579 mg, 72%).
72%	In ethanol; at 80.0℃; for 2.0h;	Compound Int-1a (733 mg, 1.33 mmol) was suspended in ethanol (10 mL) and the resulting suspension was heated to 80 C and allowed to stir for 5 minutes. Compound Int- 1b (236 mg, 1.33 mmol) was then added and the resulting reaction was allowed to stir at 80 C for an additional 2 hours. The reaction was then cooled to room temperature using in an ice bath and the reaction mixture was filtered. The collected red solid was dried under vacuum to provide compound Int-1c (579 mg, 72%).
72%	In ethanol; at 80.0℃; for 2.0h;	Compound Int-1a (733 mg, 1.33 mmol) was suspended in ethanol (10 mL) and the resulting suspension was heated to 80 C. and allowed to stir for 5 minutes. Compound Int-1b (236 mg, 1.33 mmol) was then added and the resulting reaction was allowed to stir at 80 C. for an additional 2 hours. The reaction was then cooled to room temperature using in an ice bath and the reaction mixture was filtered. The collected red solid was dried under vacuum to provide compound Int-1c (579 mg, 72%).
72%	In ethanol; at 80.0℃; for 2.0h;	Compound Int-1a (733 mg, 1.33 mmol) was taken up in ethanol (10 mL) and the resulting suspension was heated to 80 C. and allowed to stir at this temperature for 5 minutes. Compound Int-1b (236 mg, 1.33 mmol) was then added and the resulting reaction was allowed to stir at 80 C. for an additional 2 hours. The reaction was then cooled to room temperature using in an ice bath and the reaction mixture was filtered. The collected red solid was dried under vacuum to provide compound Int-1c (579 mg, 72%).

Reference： [1]Patent: WO2009/61498,2009,A1 .Location in patent: Page/Page column 102-103
[2]Patent: WO2010/91067,2010,A2 .Location in patent: Page/Page column 63-64
[3]Patent: US2010/331320,2010,A1 .Location in patent: Page/Page column 27; 28
[4]Patent: WO2011/11123,2011,A1 .Location in patent: Page/Page column 87
[5]Patent: WO2012/142085,2012,A1 .Location in patent: Page/Page column 54-55
[6]Patent: WO2014/62596,2014,A1 .Location in patent: Page/Page column 52
[7]Patent: US2014/161770,2014,A1 .Location in patent: Paragraph 0220; 0221
[8]Patent: US2014/206640,2014,A1 .Location in patent: Paragraph 0228; 0229

5
[ 351498-10-7 ]
[ 71-48-7 ]
C₃₆H₅₆CoN₂O₂ [ No CAS ]

Yield	Reaction Conditions	Operation in experiment
87%	In ethanol; at 80.0℃; for 2.0h;	N,N-Bis(3,5-di-tert-butylsalicylidene)-1 ,1 ,2,2-tetramethylethylenediamine (24, 0.73 g, 1 .3 mmol)was suspended in 10.0 mL of ethanol. The resulting suspension was heated to 80 c and stirred for 5minutes under argon balloon. Cobalt (II) acetate (0.24g, 1 .3 mmol) was then added, and the reactionmixture was stirred for another 2 hours at 80 00. The crimson red suspension was cooled down to roomtemperature in an ice bath and was filtered. The collected red solid was dried under vacuum to provide0.70 g of compound 25 (87%).

Reference： [1]Patent: WO2016/94677,2016,A2 .Location in patent: Page/Page column 44

6
[ 351498-10-7 ]
[ 71-48-7 ]
1,1,2,2-tetramethyl-1,2-ethanediamino-N,N'-bis(3,5-di-tert-butylsalicylidene) cobalt(II) [ No CAS ]

Yield	Reaction Conditions	Operation in experiment
75%	In ethanol; for 3.0h;Inert atmosphere; Reflux;	A 50 mL flask was charged with N,N?-bis(3,5-di-tert-butylsalicylidene)-1,1,2,2-tetramethylethenediamine (0.4302 g, 0.78 mmol, 1.0 equiv), EtOH (17 mL), and Co(OAc)2 (0.1385 g,0.78 mmol, 1.0 equiv). The mixture was degassed and then heated to reflux under nitrogen for 3 h,cooled to room temperature. The precipitate was filtered and the purple solid was washed with EtOH(10 mL) and dried under high vacuum to give 0.3533 g (75%) of the cobalt(II) complex.
303 mg	In ethanol; for 2.16h;Reflux; Inert atmosphere;	A suspension of <strong>[351498-10-7]N,N'-bis(3,5-di-tert-butylsalicylidene)-1,1,2,2-tetramethylethylenediamine</strong> (500 mg) in ethanol (20 mL) was refluxed under an argon atmosphere for 10 minutes. To the mixture was added cobalt (II) acetate (161 mg), and then the mixture was refluxed for 2 hours. The mixture was allowed to cool to room temperature and then the precipitate was collected by filtration. The obtained solid was washed with ethanol, and dried under reduced pressure to give the title compound (303 mg).

Reference： [1]Bioorganic and Medicinal Chemistry,2017,vol. 25,p. 3649 - 3657
[2]Patent: EP3459941,2019,A1 .Location in patent: Paragraph 0140

7
[ 351498-10-7 ]
[ 109-63-7 ]
C₃₆H₅₄B₂F₄N₂O₂ [ No CAS ]

Yield	Reaction Conditions	Operation in experiment
	With N-ethyl-N,N-diisopropylamine; In toluene; at 40.0℃; for 2.5h;Inert atmosphere;	In a nitrogen atmosphere, add to the reactor,2,2 '-[(1,1,2,2-tetramethyl-1,2-ethylenediyl) bis (nitromethyl)] bis [4,6-bis (1,1-dimethyl (Ethyl)] phenol, 16.46g (30mmol),21.6 g (152 mmol) of boron trifluoride-ether complex,300ml toluene20 g (152 mmol) of N, N-diisopropylethylamine was stirred with heating at 40 C for 2.5 hours.Cool to room temperature, add 300ml of water, and separate the filtrate into organic and aqueous layers.The organic layer was washed twice with a saturated sodium carbonate aqueous solution and dried over magnesium sulfate.The obtained solid was recrystallized from toluene (150 ml) and ethanol (750 ml),This gave 18.78 g of crude product. The crude product is under pressure 3 × 10-3Pa,Sublimation at a temperature of 225 C gave compound [69] (light yellow solid).

Reference： [1]Patent: TW2019/25212,2019,A .Location in patent: Paragraph 0112; 0113

8
[ 37942-07-7 ]
[ 75804-28-3 ]
[ 351498-10-7 ]

Yield	Reaction Conditions	Operation in experiment
	With triethylamine In ethanol for 12h; Reflux;

Reference： [1]Wu, Xiangyu; Gannett, Cara N.; Liu, Jinjian; Zeng, Rui; Novaes, Luiz F. T.; Wang, Hongsen; Abruña, Héctor D.; Lin, Song [Journal of the American Chemical Society, 2022, vol. 144, # 39, p. 17783 - 17791]

9
[ 19715-19-6 ]
[ 75804-28-3 ]
[ 351498-10-7 ]

Yield	Reaction Conditions	Operation in experiment
91 %	With triethylamine In dichloromethane Reflux;

Reference： [1]Serviano, Juan M. I.; Phipps, Erik J. T.; Holland, Patrick L. [Journal of Organic Chemistry, 2023, vol. 88, # 5, p. 3277 - 3281]

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P308 + P313	IF exposed or concerned: Get medical advice/attention.
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P332 + P313	IF SKIN irritation occurs: Get medical advice/attention.
P333 + P313	IF SKIN irritation or rash occurs: Get medical advice/attention.
P335 + P334	Brush off loose particles from skin. Immerse in cool water/wrap in wet bandages.
P337 + P313	IF eye irritation persists: Get medical advice/attention.
P342 + P311	IF experiencing respiratory symptoms: call a POISON CENTER or doctor/physician.
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H201	Explosive; mass explosion hazard
H202	Explosive; severe projection hazard
H203	Explosive; fire, blast or projection hazard
H204	Fire or projection hazard
H205	May mass explode in fire
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H221	Flammable gas
H222	Extremely flammable aerosol
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H226	Flammable liquid and vapour
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H229	Pressurized container: may burst if heated
H230	May react explosively even in the absence of air
H231	May react explosively even in the absence of air at elevated pressure and/or temperature
H240	Heating may cause an explosion
H241	Heating may cause a fire or explosion
H242	Heating may cause a fire
H250	Catches fire spontaneously if exposed to air
H251	Self-heating; may catch fire
H252	Self-heating in large quantities; may catch fire
H260	In contact with water releases flammable gases which may ignite spontaneously
H261	In contact with water releases flammable gas
H270	May cause or intensify fire; oxidizer
H271	May cause fire or explosion; strong oxidizer
H272	May intensify fire; oxidizer
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H281	Contains refrigerated gas; may cause cryogenic burns or injury
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H301	Toxic if swallowed
H302	Harmful if swallowed
H303	May be harmful if swallowed
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H310	Fatal in contact with skin
H311	Toxic in contact with skin
H312	Harmful in contact with skin
H313	May be harmful in contact with skin
H314	Causes severe skin burns and eye damage
H315	Causes skin irritation
H316	Causes mild skin irritation
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H319	Causes serious eye irritation
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H401	Toxic to aquatic life
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H411	Toxic to aquatic life with long-lasting effects
H412	Harmful to aquatic life with long-lasting effects
H413	May cause long-lasting harmful effects to aquatic life
H420	Harms public health and the environment by destroying ozone in the upper atmosphere

[ CAS No. 351498-10-7 ] {[proInfo.proName]}

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[ 351498-10-7 ] Synthesis Path-Downstream 1~9

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