[ CAS No. 3282-73-3 ] {[proInfo.proName]}

Name: 3282-73-3|Dilauryldimethylammonium Bromide|98%
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SKU: A314603
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2D 3D

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Quality Control of [ 3282-73-3 ]

COA NMR CNMR HPLC LC-MS

Related Doc. of [ 3282-73-3 ]

SDS Specification

Alternatived Products of [ 3282-73-3 ]

Product Details of [ 3282-73-3 ]

CAS No. :	3282-73-3	MDL No. :	MFCD00041969
Formula :	C₂₆H₅₆BrN	Boiling Point :	-
Linear Structure Formula :	-	InChI Key :	XRWMGCFJVKDVMD-UHFFFAOYSA-M
M.W :	462.63	Pubchem ID :	18669
Synonyms :

Safety of [ 3282-73-3 ]

Signal Word:	Warning	Class:	N/A
Precautionary Statements:	P261-P305+P351+P338	UN#:	N/A
Hazard Statements:	H315-H319-H335	Packing Group:	N/A
GHS Pictogram:

Application In Synthesis of [ 3282-73-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

Upstream synthesis route of [ 3282-73-3 ]
Downstream synthetic route of [ 3282-73-3 ]

[ 3282-73-3 ] Synthesis Path-Upstream 1~5

1
[ 143-15-7 ]
[ 124-40-3 ]
[ 112-18-5 ]
[ 3282-73-3 ]

Yield	Reaction Conditions	Operation in experiment
40%	at 20 - 25℃; for 20 h;	A mixture of a 38percent aqueous solution of dimethylamine (12.5 mL, 93.8 mmol) and dodecyl bromide (11.7 g, 46.9 mmol) in benzene (15 mL) was stirred at 20—25 °C for 20 h. Then, a 50percent aqueous solution of NaOH (1.9 g, 46.9 mmol) was added to the reaction mixture, and the resulting mixture was evaporated in vacuo. The residue was dissolved in CHCl3 (20 mL), the formed precipitate was filtered off, and the filtrate was evaporated in vacuo. According to the 1H NMR spectral data, the isolated mixture contained amine 6a (4.1 g, 40percent), N,N-didodecyl-N,N-dimethylammonium bromide (4.9 g, 46percent), and unreacted dodecyl bromide (1.7 g, 14percent).

Reference： [1] Russian Chemical Bulletin, 2014, vol. 63, # 11, p. 2445 - 2454[2] Izv. Akad. Nauk, Ser. Khim., 2014, # 11, p. 2445 - 2454

2
[ 112-18-5 ]
[ 143-15-7 ]
[ 3282-73-3 ]

Reference： [1] Chemical Communications, 2006, # 44, p. 4575 - 4577
[2] Journal of Organic Chemistry, 1984, vol. 49, # 20, p. 3774 - 3778
[3] Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1987, p. 541 - 546
[4] Journal of Physical Chemistry, 1983, vol. 87, # 4, p. 538 - 540
[5] Bulletin of the Chemical Society of Japan, 2003, vol. 76, # 10, p. 1903 - 1910
[6] Patent: WO2005/97729, 2005, A2, . Location in patent: Page/Page column 49-50; 56-57

3
[ 4536-30-5 ]
[ 3282-73-3 ]

Reference： [1] Russian Chemical Bulletin, 2014, vol. 63, # 11, p. 2445 - 2454[2] Izv. Akad. Nauk, Ser. Khim., 2014, # 11, p. 2445 - 2454

4
[ 74-83-9 ]
[ 2915-90-4 ]
[ 3282-73-3 ]

Reference： [1] Molecular Crystals and Liquid Crystals (1969-1991), 1987, vol. 146, p. 121 - 136

5
[ 23381-53-5 ]
[ 3282-73-3 ]

Reference： [1] Journal of Physical Chemistry, 1987, vol. 91, # 3, p. 674 - 685

[ 3282-73-3 ] Synthesis Path-Downstream 1~22

1
[ 74-83-9 ]
[ 2915-90-4 ]
[ 3282-73-3 ]

Reference： [1]Molecular Crystals and Liquid Crystals (1969-1991),1987,vol. 146,p. 121 - 136

2
[ 3282-73-3 ]
[ 2386-53-0 ]
Dodecane-1-sulfonatedidodecyl-dimethyl-ammonium; [ No CAS ]

Reference： [1]Bulletin of the Chemical Society of Japan,1988,vol. 61,p. 3077 - 3082

3
[ 3282-73-3 ]
[ 23381-53-5 ]

Reference： [1]Tetrahedron Letters,1984,vol. 25,p. 3765 - 3768

4
[ 3282-73-3 ]
didodecyldimethylammonium sulfate [ No CAS ]

Reference： [1]Canadian Journal of Chemistry,1988,vol. 66,p. 1566 - 1570

5
[ 23381-53-5 ]
[ 3282-73-3 ]

Reference： [1]Journal of Physical Chemistry,1987,vol. 91,p. 674 - 685

6
[ 112-18-5 ]
[ 143-15-7 ]
[ 3282-73-3 ]

Yield	Reaction Conditions	Operation in experiment
	In methanol; at 65 - 142℃;Conversion of starting material;	A 1-liter, creased, 4-necked round bottom Pyrex flask equipped with mechanical stirrer, 250-milliliter (ml) addition funnel, temperature probe, heating mantle, and water-cooled total reflux condenser was used. The flask was initially charged with 200 grams (1.08 mole) of ADMA-10 (decyldimethylamine, available from Albemarle Corporation, Baton Rouge, LA), and 239 grams (1.08 mole) decyl bromide was placed in the addition funnel. The stirrer was turned on and the reactor was heated to 65C. The decyl bromide was added dropwise to the ADMA-10 as the temperature of the reactor was allowed to rise from 65C to 142C. The addition funnel was then charged with 110 grams of methanol, and the methanol was added dropwise to the solution as the temperature of the reactor was allowed to fall to 90C. After the entire volume of the methanol was added to the reaction mixture, the heat and stirring were ceased and the intermediate quaternary ammonium (quat-Br) solution was allowed to cool.

Reference： [1]Chemical Communications,2006,p. 4575 - 4577
[2]Journal of Organic Chemistry,1984,vol. 49,p. 3774 - 3778
[3]Journal of the Chemical Society. Perkin transactions II,1987,p. 541 - 546
[4]Journal of Physical Chemistry,1983,vol. 87,p. 538 - 540
[5]Bulletin of the Chemical Society of Japan,2003,vol. 76,p. 1903 - 1910
[6]Patent: WO2005/97729,2005,A2 .Location in patent: Page/Page column 49-50; 56-57

Yield	Reaction Conditions	Operation in experiment
		EXAMPLE 10 Finsolv 116/Didodecyldimethylammonium bromide Microcapsules Microcapsules were prepared as in Example 1, except using the following materials and reaction conditions: Didodecyldimethylammonium bromide 75 grams Finsolv 116 150 grams Pre-mixing temperature 76 C. Reactor temperature 52 C. FC-77 fluid 800 ml/Cab-O-Sil TS-720 1.5 grams at 11 C.

9
[ 68494-08-6 ]
[ 3282-73-3 ]
nickel dichloride [ No CAS ]
(C₁₂H₂₅)2Me₂NNi(dmit)2 [ No CAS ]

Reference： [1]Chemistry Letters,1988,p. 1667 - 1670

10
9K⁽¹⁺⁾*BW₁₁O₃₉^(9-)=K₉[BW₁₁O₃₉] [ No CAS ]
[ 3282-73-3 ]
(dimethyl didodecylammonium)9[BW₁₁O₃₉] [ No CAS ]

Reference： [1]Journal of Physical Chemistry B,2006,vol. 110,p. 24847 - 24854

11
hydroxygallium naphthalocyaninetetrasulfonic acid [ No CAS ]
[ 3282-73-3 ]
4C₂₆H₅₆N⁽¹⁺⁾*C₄₈H₂₁GaN₈O₁₃S₄^(4-) [ No CAS ]

Yield	Reaction Conditions	Operation in experiment
39%	In water; for 0.08333330000000001h;Product distribution / selectivity;	A mixture of hydroxygallium(III) naphthalocyaninetetrasulfonic acid 4 (849 mg, 0.758 mmol) and didodecyldimethylammonium bromide (1.61 g, 3.49 mmol) in water (100 mL) was stirred for 5 min. The reaction mixture was diluted with water (100 mL) and extracted with chloroform/methanol (50:50, 2×200 mL). The combined organic layers were evaporated and the residue was suspended in warm water (200 mL), filtered, and washed with warm water and cold water/acetone (50:50) and dried to give the product 6 as a dark-green powder (777 mg, 39%).

Reference： [1]Patent: US2009/35533,2009,A1 .Location in patent: Page/Page column 22

12
4C₁₂H₂₇N*C₄₈H₂₅GaN₈O₁₃S₄ [ No CAS ]
[ 3282-73-3 ]
4C₂₆H₅₆N⁽¹⁺⁾*C₄₈H₂₁GaN₈O₁₃S₄^(4-) [ No CAS ]

Yield	Reaction Conditions	Operation in experiment
90%	In methanol;Product distribution / selectivity;	A mixture of tetrakis(tributylammonium) hydroxygallium(III) naphthalocyaninetetrasulfonate (5.74 g, 3.08 mmol) and didodecyldimethylammonium bromide (5.71 g, 0.012 mol) in methanol (200 mL) was evaporated to half volume with heating under a stream of nitrogen and diluted with water (100 mL). The solid was filtered off and washed with hot water (3×250 mL) and hot acetone/water (50:50, 3×250 mL) and allowed to dry. The solid was then washed further with toluene (2×250 mL) and boiling hexane (250 mL) and dried to give the product as a green powder (7.32 g, 90%).1H NMR (d6-DMSO) delta 0.86 (24H, t, J=6.6 Hz); 1.25 (144H, m); 1.62 (16H, m); 3.20 (16H, m); 4.25 (24H, s); 7.9-11.1 (20H, m).1H NMR (d6-DMSO): delta -0.46 (1H, s); 0.83 (24H, t, J=6.6 Hz); 1.25 (144H, m); 1.60 (16H, m); 3.20 (16H, m); 4.25 (24H, s); 7.9-11.1 (20H, m).UV-Vis-NIR (DMSO): lambdamax 790, 704, 342 nm.

Reference： [1]Patent: US2009/35533,2009,A1 .Location in patent: Page/Page column 22

13
[ 3282-73-3 ]
[ 7705-08-0 ]
[ 1373351-94-0 ]

Reference： [1]Angewandte Chemie - International Edition,2012,vol. 51,p. 2414 - 2416

14
[ 326-91-0 ]
europium(III) chloride hexahydrate [ No CAS ]
[ 3282-73-3 ]
C₃₂H₁₆EuF₁₂O₈S₄^(1-)*C₂₆H₅₆N⁽¹⁺⁾ [ No CAS ]

Reference： [1]New Journal of Chemistry,2012,vol. 36,p. 1978 - 1984

15
[ 326-91-0 ]
gadolinium(III) chloride hexahydrate [ No CAS ]
[ 3282-73-3 ]
C₃₂H₁₆F₁₂GdO₈S₄^(1-)*C₂₆H₅₆N⁽¹⁺⁾ [ No CAS ]

Reference： [1]New Journal of Chemistry,2012,vol. 36,p. 1978 - 1984

16
[ 3282-73-3 ]
[ 151-21-3 ]
didodecyldimethylammonium dodecyl sulfate [ No CAS ]

Reference： [1]Thermochimica Acta,2014,vol. 591,p. 119 - 129

17
[ 143-15-7 ]
[ 124-40-3 ]
[ 112-18-5 ]
[ 3282-73-3 ]

Yield	Reaction Conditions	Operation in experiment
40%; 46%	In water; benzene; at 20 - 25℃; for 20.0h;	A mixture of a 38% aqueous solution of dimethylamine (12.5 mL, 93.8 mmol) and dodecyl bromide (11.7 g, 46.9 mmol) in benzene (15 mL) was stirred at 20-25 C for 20 h. Then, a 50% aqueous solution of NaOH (1.9 g, 46.9 mmol) was added to the reaction mixture, and the resulting mixture was evaporated in vacuo. The residue was dissolved in CHCl3 (20 mL), the formed precipitate was filtered off, and the filtrate was evaporated in vacuo. According to the 1H NMR spectral data, the isolated mixture contained amine 6a (4.1 g, 40%), N,N-didodecyl-N,N-dimethylammonium bromide (4.9 g, 46%), and unreacted dodecyl bromide (1.7 g, 14%).

Reference： [1]Russian Chemical Bulletin,2014,vol. 63,p. 2445 - 2454
Izv. Akad. Nauk, Ser. Khim.,2014,p. 2445 - 2454

18
[ 4536-30-5 ]
[ 3282-73-3 ]

Reference： [1]Russian Chemical Bulletin,2014,vol. 63,p. 2445 - 2454
Izv. Akad. Nauk, Ser. Khim.,2014,p. 2445 - 2454

19
sodium salt of bis(5-sulfo-8-quinolinate)platinum(II) [ No CAS ]
[ 3282-73-3 ]
2C₂₆H₅₆N⁽¹⁺⁾*C₁₈H₁₀N₂O₈PtS₂^(2-) [ No CAS ]

Reference： [1]Chemistry - A European Journal,2015,vol. 21,p. 19149 - 19158

20
europioum(III) chloride [ No CAS ]
[ 3282-73-3 ]
[ 120-46-7 ]
C₆₀H₄₄EuO₈^(1-)*C₂₆H₅₆N⁽¹⁺⁾ [ No CAS ]

Reference： [1]Luminescence,2019,vol. 34,p. 877 - 886

21
europioum(III) chloride [ No CAS ]
[ 367-57-7 ]
[ 3282-73-3 ]
C₂₀H₁₆EuF₁₂O₈^(1-)*C₂₆H₅₆N⁽¹⁺⁾ [ No CAS ]

Reference： [1]Luminescence,2019,vol. 34,p. 877 - 886

22
[ 3282-73-3 ]
[ 3401-74-9 ]

Yield	Reaction Conditions	Operation in experiment
	Multi-step reaction with 2 steps 1: sodium hydroxide / ethanol / 0.25 h / 20 °C 2: hydrogenchloride / water / 24 h / Inert atmosphere

Reference： [1]Gu, Jingjing; Liu, Han; Luo, Xiliang; Qu, Yang; Wu, Zhongtao; Zhang, Lei [Journal of Molecular Liquids, 2021, vol. 337]

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Response
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P307	IF exposed:
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P310	Immediately call a POISON CENTER or doctor/physician.
P311	Call a POISON CENTER or doctor/physician.
P312	Call a POISON CENTER or doctor/physician if you feel unwell.
P313	Get medical advice/attention.
P314	Get medical advice/attention if you feel unwell.
P315	Get immediate medical advice/attention.
P320
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P321
P322
P330	Rinse mouth.
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P340	Remove victim to fresh air and keep at rest in a position comfortable for breathing.
P341	If breathing is difficult, remove victim to fresh air and keep at rest in a position comfortable for breathing.
P342	If experiencing respiratory symptoms:
P350	Gently wash with plenty of soap and water.
P351	Rinse cautiously with water for several minutes.
P352	Wash with plenty of soap and water.
P353	Rinse skin with water/shower.
P360	Rinse immediately contaminated clothing and skin with plenty of water before removing clothes.
P361	Remove/Take off immediately all contaminated clothing.
P362	Take off contaminated clothing and wash before reuse.
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P371	In case of major fire and large quantities:
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P378
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P391	Collect spillage. Hazardous to the aquatic environment
P301 + P310	IF SWALLOWED: Immediately call a POISON CENTER or doctor/physician.
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P301 + P330 + P331	IF SWALLOWED: Rinse mouth. Do NOT induce vomiting.
P302 + P334	IF ON SKIN: Immerse in cool water/wrap in wet bandages.
P302 + P350	IF ON SKIN: Gently wash with plenty of soap and water.
P303 + P361 + P353	IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.
P304 + P312	IF INHALED: Call a POISON CENTER or doctor/physician if you feel unwell.
P304 + P340	IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P304 + P341	IF INHALED: If breathing is difficult, remove victim to fresh air and keep at rest in a position comfortable for breathing.
P305 + P351 + P338	IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing.
P306 + P360	IF ON CLOTHING: Rinse Immediately contaminated CLOTHING and SKIN with plenty of water before removing clothes.
P307 + P311	IF exposed: call a POISON CENTER or doctor/physician.
P308 + P313	IF exposed or concerned: Get medical advice/attention.
P309 + P311	IF exposed or if you feel unwell: call a POISON CENTER or doctor/physician.
P332 + P313	IF SKIN irritation occurs: Get medical advice/attention.
P333 + P313	IF SKIN irritation or rash occurs: Get medical advice/attention.
P335 + P334	Brush off loose particles from skin. Immerse in cool water/wrap in wet bandages.
P337 + P313	IF eye irritation persists: Get medical advice/attention.
P342 + P311	IF experiencing respiratory symptoms: call a POISON CENTER or doctor/physician.
P370 + P376	In case of fire: Stop leak if safe to Do so.
P370 + P378	In case of fire:
P370 + P380	In case of fire: Evacuate area.
P370 + P380 + P375	In case of fire: Evacuate area. Fight fire remotely due to the risk of explosion.
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H200	Unstable explosive
H201	Explosive; mass explosion hazard
H202	Explosive; severe projection hazard
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H242	Heating may cause a fire
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H411	Toxic to aquatic life with long-lasting effects
H412	Harmful to aquatic life with long-lasting effects
H413	May cause long-lasting harmful effects to aquatic life
H420	Harms public health and the environment by destroying ozone in the upper atmosphere

[ CAS No. 3282-73-3 ] {[proInfo.proName]}

Quality Control of [ 3282-73-3 ]

Related Doc. of [ 3282-73-3 ]

Product Details of [ 3282-73-3 ]

Safety of [ 3282-73-3 ]

Application In Synthesis of [ 3282-73-3 ]

[ 3282-73-3 ] Synthesis Path-Upstream 1~5

[ 3282-73-3 ] Synthesis Path-Downstream 1~22

Precautionary Statements-General

Prevention

Response

Storage

Disposal

Physical hazards

Health hazards

Environmental hazards

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