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Chemistry
Heterocyclic Building Blocks
Imidazolines
1-(p-Tolyl)-1H-imidazole-2(3H)-thione
Chemistry
Heterocyclic Building Blocks
Organic Building Blocks
Imidazolines
Aryls Amides Aliphatic Heterocycles

[ CAS No. 23671-38-7 ] {[proInfo.proName]}

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Chemical Structure| 23671-38-7
Chemical Structure| 23671-38-7
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Product Details of [ 23671-38-7 ]

CAS No. :23671-38-7 MDL No. :MFCD02948427
Formula : C10H10N2S Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 190.27 Pubchem ID :-
Synonyms :

Safety of [ 23671-38-7 ]

Signal Word: Class:
Precautionary Statements: UN#:
Hazard Statements: Packing Group:

Application In Synthesis of [ 23671-38-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 23671-38-7 ]

[ 23671-38-7 ] Synthesis Path-Downstream   1~6

  • 1
  • [ 3347-62-4 ]
  • [ 23671-38-7 ]
  • K(1+)*[HB(C3H2N2(S)(CH3C6H4))2(C3HN2(CH3)C6H5)](1-)=K[HB(C3H2N2(S)(CH3C6H4))2(C3HN2(CH3)C6H5)] [ No CAS ]
Reference： [1]European Journal of Inorganic Chemistry,2003,p. 2502 - 2511
  • 2
  • potassium borohydride [ No CAS ]
  • [ 3347-62-4 ]
  • [ 23671-38-7 ]
  • K(1+)*[HB(C3H2N2(S)(CH3C6H4))2(C3HN2(CH3)C6H5)](1-)=K[HB(C3H2N2(S)(CH3C6H4))2(C3HN2(CH3)C6H5)] [ No CAS ]
Reference： [1]European Journal of Inorganic Chemistry,2003,p. 2502 - 2511
  • 3
  • [ 90560-54-6 ]
  • [ 23671-38-7 ]
  • [ 1187945-92-1 ]
YieldReaction ConditionsOperation in experiment
74.1% With sodium carbonate In N,N-dimethyl-formamide
Reference： [1]Location in patent: experimental part Zhan, Peng; Liu, Xinyong; Zhu, Junjie; Fang, Zengjun; Li, Zhenyu; Pannecouque, Christophe; Clercq, Erik De [Bioorganic and Medicinal Chemistry, 2009, vol. 17, # 16, p. 5775 - 5781]
  • 4
  • [ 347-66-0 ]
  • [ 23671-38-7 ]
  • [ 1187945-89-6 ]
YieldReaction ConditionsOperation in experiment
88% With sodium carbonate In N,N-dimethyl-formamide
Reference： [1]Location in patent: experimental part Zhan, Peng; Liu, Xinyong; Zhu, Junjie; Fang, Zengjun; Li, Zhenyu; Pannecouque, Christophe; Clercq, Erik De [Bioorganic and Medicinal Chemistry, 2009, vol. 17, # 16, p. 5775 - 5781]
  • 5
  • [ 3347-62-4 ]
  • [ 23671-38-7 ]
  • [(HB(C3H2N2(S)C6H4CH3)2(C3HN2(CH3)C6H5))2Zn] [ No CAS ]
Reference： [1]European Journal of Inorganic Chemistry,2003,p. 2502 - 2511
  • 6
  • [ 16971-33-8 ]
  • [ 23671-38-7 ]
  • RuH(κ2-S,N-1-(4-methylphenyl)imidazole-2-thione-H)(CO)(PPh3)2 [ No CAS ]
YieldReaction ConditionsOperation in experiment
50% With sodium methylate In tetrahydrofuran at 20℃; for 2h; Schlenk technique; Synthesis of [RuH(κ2-S,N-imtMPh)(CO)(PPh3)2] (4a) To a slurry of HimtMPh (19 mg, 0.10 mM) and MeONa (5.4 mg, 0.10 mM) in THF (5 mL)was added a solution of [RuHCl(CO)(PPh3)3] (95 mg, 0.10 mM) in THF (10 mL). The mixturewas stirred for 2 h at room temperature. The solvent was removed in vacuo, and theresidue was washed with hexane and further recrystallized from CH2Cl2/hexane at room temperature. Yellow crystalline product of 4a was obtained in three days. Yield: 42 mg,50%. 31P NMR (CDCl3): 39.3 (s) ppm. 1H NMR (CDCl3): 14.30 (t, RuH, J = 22.5 Hz,1H), 2.30 (s, Me, 3H), 6.04 (d, im-CH, J = 2.0 Hz, 1H), 6.37 (d, im-CH, J = 2.0 Hz, 1H),6.68 (d, C6H4, 2H, J = 8.4 Hz), 7.10 (d, C6H4, 2H, J = 8.8 Hz), 7.32-7.58 (m2, PC6H5,30H) ppm. IR (KBr disk, cm1): 1927 (vs), 1593 (m), 1565 (m), 1503 (s), 1436 (s), 1321(m), 1264 (s), 1098 (s), 1021 (s), 801 (s), 746 (s), 697 (s), 540 (s), 524 (s), 502 (s). MS(FAB): m/z 844 [M+], 842 [M+ - H - 1], 808 [M+ - H - Cl], 814 [Ru(κ2-S,N-imtMPh)(PPh3)2]+, 552 [Ru(κ2-S,N-imtMPh)(PPh3)]+, 291 [Ru(κ2-S,N-imtMPh)]+. Anal. Calcd forC47H40N2OP2SRu (%): C, 66.89; H, 4.78; N, 3.32. Found: C, 66.79; H, 4.76; N, 3.35
Reference： [1]Qin, Yi; Ma, Qing; Jia, Ai-Quan; Chen, Qun; Zhang, Qian-Feng [Journal of Coordination Chemistry, 2013, vol. 66, # 8, p. 1405 - 1415]

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