Home Cart 0 Sign in  

[ CAS No. 23632-70-4 ] {[proInfo.proName]}

,{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]}
Chemical Structure| 23632-70-4
Chemical Structure| 23632-70-4
Structure of 23632-70-4 * Storage: {[proInfo.prStorage]}
Cart0 Add to My Favorites Add to My Favorites Bulk Inquiry Inquiry Add To Cart

Quality Control of [ 23632-70-4 ]

Related Doc. of [ 23632-70-4 ]

Alternatived Products of [ 23632-70-4 ]

Product Details of [ 23632-70-4 ]

CAS No. :23632-70-4 MDL No. :MFCD00038885
Formula : C28H44N2O6 Boiling Point : -
Linear Structure Formula :- InChI Key :JEGXFHMMFLKBBW-YDALLXLXSA-N
M.W : 504.66 Pubchem ID :52974253
Synonyms :

Safety of [ 23632-70-4 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P305+P351+P338-P330-P332+P313-P337+P313-P362-P403+P233-P405-P501 UN#:N/A
Hazard Statements:H302-H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 23632-70-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 23632-70-4 ]

[ 23632-70-4 ] Synthesis Path-Downstream   1~20

  • 1
  • [ 623-33-6 ]
  • [ 23632-70-4 ]
  • [ 21611-61-0 ]
YieldReaction ConditionsOperation in experiment
With dicyclohexyl-carbodiimide
  • 2
  • [ 27486-72-2 ]
  • [ 23632-70-4 ]
YieldReaction ConditionsOperation in experiment
93% With tetrabutyl ammonium fluoride In tetrahydrofuran Ambient temperature;
  • 3
  • [ 6306-52-1 ]
  • [ 23632-70-4 ]
  • [ 90982-89-1 ]
YieldReaction ConditionsOperation in experiment
With dicyclohexyl-carbodiimide In dichloromethane -20 deg C, 1 h, then r.t. 3 h;
  • 5
  • (S)-tryptophan methyl ester hydrochloride [ No CAS ]
  • [ 23632-70-4 ]
  • [ 98385-60-5 ]
YieldReaction ConditionsOperation in experiment
100% With dicyclohexyl-carbodiimide In dichloromethane Ambient temperature; overnight;
95% With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 1h; 40 Preparation of compound Cbz-Asp(OtBu)-Trp-OMe:341mg (1mmol) Z-Asp(OtBu)-OHAnd 254mg (1mmol) H-Trp-OMe.HCl addedIn 3ml DMF solvent,Add 286mg (1.5mmol) EDC.HCl to it,202mg (1.5mmol) HOBT,494μL (1.5mmol) DIEA,Reaction at room temperature for 1 hour,After the reaction,Add 60ml ethyl acetate to the reaction solution successively,50ml 5% (volume fraction) phosphoric acid aqueous solution,50ml saturated NaHCO3 aqueous solution,50ml water and 50ml saturated NaCl aqueous solution were extracted once, and the organic layer was dried with anhydrous sodium sulfate,Filter and evaporate to dryness under reduced pressure,Thus, 496.8 mg of pure compound Cbz-Asp(OtBu)-Trp-OMe was obtained, and the yield was 95%.
  • 6
  • [ 23632-70-4 ]
  • (S)-2-((S)-2-Amino-3-tert-butoxycarbonyl-propionylamino)-3-methyl-butyric acid methyl ester; hydrochloride [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: dicyclohexylcarbodiimide / CH2Cl2 / -20 deg C, 1 h, then r.t. 3 h 2: H2, HCl / 5percent Pd/C / methanol / 3 h / Ambient temperature
  • 7
  • [ 23632-70-4 ]
  • (S)-3-Amino-N-[(S)-2-(1H-indol-3-yl)-1-methoxycarbonyl-ethyl]-succinamic acid tert-butyl ester; hydrochloride [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: 100 percent / dicyclohexylcarbodiimide / CH2Cl2 / Ambient temperature; overnight 2: H2, HCl / 5percent Pd/C / methanol / 1.5 h / Ambient temperature
  • 8
  • [ 23632-70-4 ]
  • [ 102837-86-5 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 3 steps 1: 100 percent / dicyclohexylcarbodiimide / CH2Cl2 / Ambient temperature; overnight 2: H2, HCl / 5percent Pd/C / methanol / 1.5 h / Ambient temperature 3: triethylamine / dimethylformamide; dioxane / 24 h / 0 °C
  • 9
  • [ 23632-70-4 ]
  • Boc-Ser-Ser-Asp(OBu-t)-Trp-N2H3 [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 4 steps 1: 100 percent / dicyclohexylcarbodiimide / CH2Cl2 / Ambient temperature; overnight 2: H2, HCl / 5percent Pd/C / methanol / 1.5 h / Ambient temperature 3: triethylamine / dimethylformamide; dioxane / 24 h / 0 °C 4: 82.5 percent / 100percent hydrazine hydrate / methanol / 2.5 h / Ambient temperature
  • 10
  • [ 23632-70-4 ]
  • [ 102837-82-1 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 3 steps 1: dicyclohexylcarbodiimide / CH2Cl2 / -20 deg C, 1 h, then r.t. 3 h 2: H2, HCl / 5percent Pd/C / methanol / 3 h / Ambient temperature 3: triethylamine / dimethylformamide; dioxane / 72 h / 0 °C
  • 11
  • [ 23632-70-4 ]
  • [ 102837-67-2 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 4 steps 1: dicyclohexylcarbodiimide / CH2Cl2 / -20 deg C, 1 h, then r.t. 3 h 2: H2, HCl / 5percent Pd/C / methanol / 3 h / Ambient temperature 3: triethylamine / dimethylformamide; dioxane / 72 h / 0 °C 4: 71.6 percent / 100percent hydrazine hydrate / methanol / 2 h / Ambient temperature
  • 12
  • [ 23632-70-4 ]
  • [ 27446-41-9 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: 92 percent 2: 1) hydrogen; 2) triethylamine; / Pd black / 1) CH3OH, HCl, dioxane; 2) DMF, 18-20 deg C, 24 h.
  • 13
  • [ 23632-70-4 ]
  • [ 103678-20-2 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 3 steps 1: 92 percent 2: 1) hydrogen; 2) triethylamine; / Pd black / 1) CH3OH, HCl, dioxane; 2) DMF, 18-20 deg C, 24 h.
  • 14
  • [ 23632-70-4 ]
  • [ 103678-21-3 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 4 steps 1: 92 percent 2: 1) hydrogen; 2) triethylamine; / Pd black / 1) CH3OH, HCl, dioxane; 2) DMF, 18-20 deg C, 24 h. 4: 94 percent / hydrazine hydrate / methanol; dimethylformamide / 10 h / 20 - 24 °C
  • 15
  • [ 23632-70-4 ]
  • [ 126027-22-3 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: DCC 2: H2 / Pd-C
  • 16
  • [ 1192373-39-9 ]
  • [ 23632-70-4 ]
  • C28H44N4O9 [ No CAS ]
YieldReaction ConditionsOperation in experiment
Stage #1: DCHA salt of the β-tert-butyl ester of N-benzyloxycarbonylaspartic acid With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In acetonitrile at 25℃; for 1h; Inert atmosphere; Stage #2: (S)-(3-(tert-butoxy)-1-hydrazino-1-oxopropan-2-yl)carbamic acid tert-butyl ester In acetonitrile at 25℃; for 8h; Inert atmosphere;
  • 17
  • [ 1262482-79-0 ]
  • [ 23632-70-4 ]
  • C25H40N4O7 [ No CAS ]
YieldReaction ConditionsOperation in experiment
Stage #1: DCHA salt of the β-tert-butyl ester of N-benzyloxycarbonylaspartic acid With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In acetonitrile at 25℃; for 1h; Inert atmosphere; Stage #2: C9H21N3O2 In acetonitrile at 25℃; for 8h; Inert atmosphere;
  • 18
  • [ 2592-20-3 ]
  • [ 23632-70-4 ]
  • C32H51N5O10 [ No CAS ]
YieldReaction ConditionsOperation in experiment
Stage #1: DCHA salt of the β-tert-butyl ester of N-benzyloxycarbonylaspartic acid With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In acetonitrile at 25℃; for 1h; Inert atmosphere; Stage #2: Nα,Nε-Di-tert.-butyloxycarbonyl-L-lysin-hydrazid In acetonitrile at 25℃; for 8h; Inert atmosphere;
  • 19
  • [ 95485-98-6 ]
  • [ 23632-70-4 ]
  • C34H48N4O9 [ No CAS ]
YieldReaction ConditionsOperation in experiment
Stage #1: DCHA salt of the β-tert-butyl ester of N-benzyloxycarbonylaspartic acid With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In acetonitrile at 25℃; for 1h; Inert atmosphere; Stage #2: N-tert.-Butyloxycarbonyl-O-tert.-butyl-L-tyrosinhydrazid In acetonitrile at 25℃; for 8h; Inert atmosphere;
  • 20
  • (S)-tryptophan methyl ester hydrochloride [ No CAS ]
  • [ 23632-70-4 ]
  • C29H32F3N3O7 [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 1 h / 20 °C 2: fluorescein / N,N-dimethyl-formamide; water / 8 h / 20 °C / Irradiation
Same Skeleton Products
Historical Records

Related Functional Groups of
[ 23632-70-4 ]

Amino Acid

Chemical Structure| 71449-08-6

[ 71449-08-6 ]

Z-D-Asp(OtBu)-OH

Similarity: 0.96