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CAS No. : | 18684-24-7 | MDL No. : | MFCD00037349 |
Formula : | C10H16N2O4 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 228.25 | Pubchem ID : | - |
Synonyms : |
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Signal Word: | Warning | Class: | |
Precautionary Statements: | P501-P270-P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313-P301+P312+P330 | UN#: | |
Hazard Statements: | H302-H315-H319 | Packing Group: | |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
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With methanol; palladium; acetic acid Hydrogenation; |
Yield | Reaction Conditions | Operation in experiment |
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With pig kidney aminopeptidase P; manganese(ll) chloride at 37℃; |
Yield | Reaction Conditions | Operation in experiment |
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1.57 g | for 1h; Cooling with ice; | 1 Preparation ofacetyl Pro-Hyp 2.28 g of Pro-Hyp (manufactured by Maruni Oil) was added little by little to 3.06 g of ice-cooled acetic anhydride (manufactured by Nacalai Tesque), and the mixture was stirred for 1 hour after completion of the addition.The solvent of the reaction product was distilled off under reduced pressure, and the solidified residue was washed with a small amount of ethyl acetate by cooling.After leaving still, the ethyl acetate was removed and recrystallized from isopropanol to obtain the desired product.(1.57g) |
Yield | Reaction Conditions | Operation in experiment |
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With acetic acid at 50 - 60℃; | 2 Preparation ofsuccinyl Pro-Hyp 4.7 g of Pro-Hyp (manufactured by Maruni Oil) and succinic anhydride (manufactured by Nacalai Tesque, 4.0 g) were dissolved in 40 mL of acetic acid (manufactured by Nacalai Tesque).The solution was heated to 50-60 ° C. and the solvent evaporated to crystallize.Next, the crystallized white precipitate was collected and recrystallized with a mixed solution of 20 mL of ethyl acetate and 20 mL of methanol.The precipitate was crushed in a mortar and dried to obtain N-succinyl Pro-Hyp powder. |