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CAS No. : | 185428-55-1 | MDL No. : | MFCD28043790 |
Formula : | C12H16N2O5 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | IGYXAKCOMRSREX-UHFFFAOYSA-N |
M.W : | 268.27 | Pubchem ID : | 10199249 |
Synonyms : |
|
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P280-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H302 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
75% | With sodium methylate In methanol; toluene | Example 4 N-(5-Methoxy-2-nitrophenyl)carbamic Acid t-butyl Ester To a solution of N-(5-methoxy-2-nitrophenyl)-N-t-butoxycarbonylcarbamic acid t-butyl ester (10.6 g) in toluene (5 ml) and methanol (30 ml) was added 24percent sodium methoxide in methanol (3.1 ml) and the mixture was stirred at 25° C. for 3 hours. At the end of this time the reaction mixture was cooled to 0° C. and the precipitated crystals were filtered to give the title compound (5.8 g, yield 75percent). IR spectrum (KBr, ν cm): 1737, 1615, 1592, 1338, 1279, 1252, 1147. 1H-NMR spectrum (CDCl3, 400 MHz, δ ppm): 1.54(9H, s), 3.91(3H, s), 6.57(1H, dd, J=9.5, 2.8 Hz), 8.16(1H, d, J=2.8 Hz), 8.18(1H, d, J=9.5 Hz). |
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