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Quality Control of [ 141045-26-3 ]

COA NMR CNMR HPLC LC-MS

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Product Details of [ 141045-26-3 ]

CAS No. :	141045-26-3	MDL No. :	MFCD23135292
Formula :	C₂₂H₁₈N₄	Boiling Point :	-
Linear Structure Formula :	-	InChI Key :	-
M.W :	338.41	Pubchem ID :	-
Synonyms :

Safety of [ 141045-26-3 ]

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Application In Synthesis of [ 141045-26-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

Downstream synthetic route of [ 141045-26-3 ]

[ 141045-26-3 ] Synthesis Path-Downstream 1~45

1
[ 121-91-5 ]
[ 25148-68-9 ]
[ 141045-26-3 ]

Reference： [1]Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical and Analytical,1993,vol. 32,p. 33 - 38

2
[ 29914-81-6 ]
[ 74-88-4 ]
[ 141045-26-3 ]

Reference： [1]Journal of the American Chemical Society,1992,vol. 114,p. 4230 - 4237
[2]Organic and Biomolecular Chemistry,2016,vol. 14,p. 8232 - 8236

3
[ 121-91-5 ]
[ 4760-34-3 ]
[ 141045-26-3 ]

Yield	Reaction Conditions	Operation in experiment
54%	With polyphosphoric acid; at 100 - 200℃; for 19h;	Isophthalic acid in an amount of 18 mmol (3.0 g) and N-methyl-1,2-phenylenediamine in an amount of 36 mmol (4.4 g) were placed into an eggplant type flask with a capacity of 500 milliliter and added polyphosphoric acid in an amount of 75 milliliter. The resultant solution reacted at the temperature of 100 C for 15 hours and further, it was heated at the temperature of 200 C for 4 hours. After the resultant solution was cooled by leaving it standing, it was added to 600 milliliter of pure water and then, the resultant solution was neutralized with NaOH aqueous solution of 5M until it became pH7, subsequently gathering a precipitated purple solid by filtration, the purple solid was washed with pure water thoroughly. The resultant solid was re-crystallized with the use of methanol and as a result, 3.3 g of aimed mbib was obtained (yield: 54 %).

Reference： [1]Inorganic Chemistry,2012,vol. 51,p. 890 - 899
[2]Patent: EP1816134,2007,A1 .Location in patent: Page/Page column 25

4
iridium(III) chloride [ No CAS ]
[ 141045-26-3 ]
[Ir(2,6-bis(N-methyl-benzimidazol-2-yl)phenyl-κC1)Cl2]2 [ No CAS ]

Yield	Reaction Conditions	Operation in experiment
	In methanol; for 5h;Heating / reflux;	Iridic chloride in an amount of 0.27 mmol (0.1 g), mbib in an amount of 0.54 mmol (0.18 g) and methanol in an amount of 15 milliliter were placed into an eggplant type flask having a capacity of 100 milliliter, and the resultant solution was refluxed with heating for 5 hours under the atmospheric nitrogen gas flow. After the resultant solution was cooled by leaving it standing, a precipitate was collected by filtration, the precipitate was washed with the use of methanol and ether, followed by drying and as a result, yellow powders were obtained. The yellow powders were identified by means of Matrix Assisted Laser Desorption/Ionization-time of flight type Mass Spectrometry apparatus (MALDI-MS), and it was confirmed that they were the aimed substance.

Reference： [1]Patent: EP1816134,2007,A1 .Location in patent: Page/Page column 25

5
Co(II) iodide*6H₂O [ No CAS ]
[ 141045-26-3 ]
CoI₂(1,3-bis(N-methyl-2-benzimidazyl)benzene) [ No CAS ]

Reference： [1]Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical and Analytical,1993,vol. 32,p. 33 - 38

6
cobalt(II) perchlorate [ No CAS ]
[ 141045-26-3 ]
{Co(1,3-bis(N-methyl-2-benzimidazyl)benzene)2}(ClO₄)2 [ No CAS ]

Reference： [1]Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical and Analytical,1993,vol. 32,p. 33 - 38

7
cobalt(II) bromide hexahydrate [ No CAS ]
[ 141045-26-3 ]
CoBr₂(1,3-bis(N-methyl-2-benzimidazyl)benzene) [ No CAS ]

Reference： [1]Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical and Analytical,1993,vol. 32,p. 33 - 38

8
cobalt(II) chloride hexahydrate [ No CAS ]
[ 141045-26-3 ]
CoCl₂(1,3-bis(N-methyl-2-benzimidazyl)benzene) [ No CAS ]

Reference： [1]Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical and Analytical,1993,vol. 32,p. 33 - 38

9
[ 14057-91-1 ]
[ 141045-26-3 ]
Cu₂(C₆H₄(CNC₆H₄NCH₃)2)2⁽²⁺⁾*2ClO₄^(1-)={Cu₂(C₆H₄(CNC₆H₄NCH₃)2)2}(ClO₄)2 [ No CAS ]

Reference： [1]Journal of the American Chemical Society,1992,vol. 114,p. 4230 - 4237

10
[ 3375-31-3 ]
[ 141045-26-3 ]
[Pd₃((CH₃NCNC₆H₄)2C₆H₃)3(OOCCH₃)3] [ No CAS ]

Reference： [1]Angewandte Chemie,1993,vol. 105,p. 432 - 434

11
dipropionatopalladium(II) [ No CAS ]
[ 7732-18-5 ]
[ 141045-26-3 ]
[Pd((CH₃NCNC₆H₄)2C₆H₃)(OOCC₂H₅)] [ No CAS ]
[Pd((CH₃NCNC₆H₄)2C₆H₃)(OOCC₂H₅)]3*H₂O [ No CAS ]

Reference： [1]Inorganic Chemistry,2001,vol. 40,p. 1826 - 1832

12
nickel(II) bromide hydrate [ No CAS ]
[ 141045-26-3 ]
[ 650600-44-5 ]

Reference： [1]Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical and Analytical,2003,vol. 42,p. 1856 - 1860

13
nickel(II) dichloride hydrate [ No CAS ]
[ 141045-26-3 ]
[ 650600-43-4 ]

Reference： [1]Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical and Analytical,2003,vol. 42,p. 1856 - 1860

14
nickel(II) iodide hydrate [ No CAS ]
[ 141045-26-3 ]
[ 67-64-1 ]
[NiI₂(1,3-bis(1-methylbenzimidazol-2-yl)benzene)(H₂O)] [ No CAS ]

Reference： [1]Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical and Analytical,2003,vol. 42,p. 1856 - 1860

15
zinc(II) chloride dihydrate [ No CAS ]
[ 141045-26-3 ]
Zn(1,3-bis(1-methylbenzimidazol-2-yl)benzene)Cl₂H₂O [ No CAS ]

Reference： [1]Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry,2003,vol. 33,p. 1207 - 1220

16
nickel(II) perchlorate hydrate [ No CAS ]
[ 141045-26-3 ]
[ 650600-47-8 ]

Reference： [1]Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical and Analytical,2003,vol. 42,p. 1856 - 1860

17
[ 141045-26-3 ]
zinc dibromide [ No CAS ]
Zn(1,3-bis(1-methylbenzimidazol-2-yl)benzene)Br₂H₂O [ No CAS ]

Reference： [1]Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry,2003,vol. 33,p. 1207 - 1220

18
[ 141045-26-3 ]
zinc(II) iodide [ No CAS ]
Zn(1,3-bis(1-methylbenzimidazol-2-yl)benzene)I₂H₂O [ No CAS ]

Reference： [1]Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry,2003,vol. 33,p. 1207 - 1220

19
zinc(II) perchlorate hydrate [ No CAS ]
[ 141045-26-3 ]
Zn(1,3-bis(1-methylbenzimidazol-2-yl)benzene)2H₂O perchlorate monohydrate [ No CAS ]

Reference： [1]Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry,2003,vol. 33,p. 1207 - 1220

20
copper(II) choride dihydrate [ No CAS ]
[ 141045-26-3 ]
[ 850309-93-2 ]

Reference： [1]Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry,2004,vol. 34,p. 1721 - 1735

21
[ 10049-07-7 ]
[ 141045-26-3 ]
[ 250579-45-4 ]

Reference： [1]Polyhedron,1999,vol. 18,p. 2351 - 2360

22
[ 141045-26-3 ]
cadmium(II) iodide [ No CAS ]
[ 838824-62-7 ]

Reference： [1]Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical and Analytical,2004,vol. 43,p. 1863 - 1867

23
[ 141045-26-3 ]
[ 10108-64-2 ]
[(CdCl₂)2(1,3-bis(1-methylbenzimidazol-2-yl)benzene)] [ No CAS ]

Reference： [1]Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical and Analytical,2004,vol. 43,p. 1863 - 1867

24
[ 15608-29-4 ]
[ 141045-26-3 ]
[ 250579-46-5 ]

Reference： [1]Polyhedron,1999,vol. 18,p. 2351 - 2360

25
cadmium(II) perchlorate hexahydrate [ No CAS ]
[ 141045-26-3 ]
[Cd(1,3-bis(1-methylbenzimidazol-2-yl)benzene)2(H₂O)](ClO₄)2*H₂O [ No CAS ]

Reference： [1]Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical and Analytical,2004,vol. 43,p. 1863 - 1867

26
copper(II) perchlorate hydrate [ No CAS ]
[ 141045-26-3 ]
[Cu(H₂O)(1,3-bis(1-methylbenzimidazol-2-yl)benzene)](ClO₄)2 [ No CAS ]

Reference： [1]Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry,2004,vol. 34,p. 1721 - 1735

27
[ 141045-26-3 ]
cadmium(II) bromide [ No CAS ]
[ 838824-61-6 ]

Reference： [1]Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical and Analytical,2004,vol. 43,p. 1863 - 1867

28
[ 141045-26-3 ]
[ 7789-45-9 ]
[ 850309-95-4 ]

Reference： [1]Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry,2004,vol. 34,p. 1721 - 1735

29
ammonium hexafluorophosphate [ No CAS ]
[ 187244-98-0 ]
[ 60-29-7 ]
[ 141045-26-3 ]
[ 75-05-8 ]
[Ir(2,6-bis(1-methyl-benzimidazol-2-yl)pyridine)(1,3-bis(1-methyl-benzimidazol-2-yl)benzene^(1-))](PF₆)2*CH₃CN*1.5(C₂H₅)2O [ No CAS ]

Reference： [1]Inorganic Chemistry,2005,vol. 44,p. 4737 - 4746

30
copper(II) perchlorate hexahydrate [ No CAS ]
[ 80937-33-3 ]
[ 141045-26-3 ]
[ 68-12-2 ]
bis[2,6-bis(1-methyl-1H-benzimidazol-2-yl)phenolate]bis(dimethylformamide)dicopper(II) perchlorate dimethylformamide tetrasolvate [ No CAS ]

Reference： [1]Helvetica Chimica Acta,2006,vol. 89,p. 841 - 853

31
copper(II) perchlorate hexahydrate [ No CAS ]
[ 7722-84-1 ]
[ 141045-26-3 ]
bis[2,6-bis(1-methyl-1H-benzimidazol-2-yl)phenolate]dicopper(II) [ No CAS ]

Reference： [1]Helvetica Chimica Acta,2006,vol. 89,p. 841 - 853

32
iridium(III) trichloride tetrahydrate [ No CAS ]
[ 141045-26-3 ]
[Ir(2,6-bis(N-methyl-benzimidazol-2-yl)phenyl-κC1)Cl2]2 [ No CAS ]

Reference： [1]Inorganic Chemistry,2006,vol. 45,p. 8907 - 8921

33
[ 17084-13-8 ]
[ 178555-66-3 ]
[ 141045-26-3 ]
[Ru(1,3-bis(1-methylbenzimidazol-2-yl)benzene(-1H))(2,6-bis(1-methylbenzimidazol-2-yl)pyridine)]PF₆*H₂O [ No CAS ]

Reference： [1]Inorganic Chemistry,2012,vol. 51,p. 890 - 899

34
[ 17084-13-8 ]
[ 72905-30-7 ]
[ 141045-26-3 ]
[ 1353653-97-0 ]

Reference： [1]Inorganic Chemistry,2012,vol. 51,p. 890 - 899

35
[ 17084-13-8 ]
[ 1438273-18-7 ]
[ 141045-26-3 ]
[Os(1,3-bis(N-methylbenzimidazolyl)benzene^(1-))(2,6-bis(N-methylbenzimidazolyl)pyridine)](PF₆)₂ [ No CAS ]

Reference： [1]Inorganic Chemistry,2013,vol. 52,p. 6464 - 6472

36
[ 17084-13-8 ]
[Ru(5,5''-divinyl-4'-(p-tolyl)-2,2':6',2''-terpyridine)Cl₃] [ No CAS ]
[ 141045-26-3 ]
[(5,5''-divinyl-4'-(p-tolyl)-2,2':6',2''-terpyridine)Ru(1,3-bis(N-methylbenzimidazolyl)benzene(-H))]PF₆ [ No CAS ]

Reference： [1]Dalton Transactions,2013,vol. 42,p. 14125 - 14133

37
[ 17084-13-8 ]
Cl2(EtOH)Os(tetrapyridylpyrazine)RuCl3 [ No CAS ]
[ 141045-26-3 ]
2F₆P^(1-)*C₆₈H₅₀N₁₄Os₂⁽²⁺⁾ [ No CAS ]

Reference： [1]Organometallics,2014,vol. 33,p. 4893 - 4904

38
[ 17084-13-8 ]
Cl2(EtOH)Ru(tetrapyridylpyrazine)RuCl3 [ No CAS ]
[ 141045-26-3 ]
2F₆P^(1-)*C₆₈H₅₀N₁₄Ru₂⁽²⁺⁾ [ No CAS ]

Reference： [1]Organometallics,2014,vol. 33,p. 4893 - 4904

39
[ 17084-13-8 ]
[ 330680-47-2 ]
[ 141045-26-3 ]
C₄₃H₃₄N₇O₆Ru⁽¹⁺⁾*F₆P^(1-) [ No CAS ]

Reference： [1]RSC Advances,2015,vol. 5,p. 90001 - 90009

40
[ 121-91-5 ]
N,N'-dimethyl-1,2-benzenediamine dihydrochloride [ No CAS ]
[ 141045-26-3 ]

Reference： [1]RSC Advances,2015,vol. 5,p. 90001 - 90009

41
[ 17084-13-8 ]
[Ru(2,6-bis(benzimidazol-2-yl)pyridine)(CH₃CN)Cl₂] [ No CAS ]
[ 141045-26-3 ]
[Ru(2,6-bis(benzimidazol-2-yl)pyridine)(2,6-bis(1-methylbenzimidazol-2-yl)benzene)][PF₆]₂ [ No CAS ]

Reference： [1]Inorganic Chemistry,2017,vol. 56,p. 6419 - 6428

42
iridium(III) chloride tetrahydrate [ No CAS ]
[ 141045-26-3 ]
[Ir(2,6-bis(N-methyl-benzimidazol-2-yl)phenyl-κC1)Cl2]2 [ No CAS ]

Reference： [1]Journal of Organometallic Chemistry,2017,vol. 845,p. 189 - 195

43
[ 141045-26-3 ]
[Ir(III)(1,3-bis(N-methylbenzimidazolyl)benzene(-1H))(2-phenylpyridine(-1H))Cl] [ No CAS ]

Reference： [1]Journal of Organometallic Chemistry,2017,vol. 845,p. 189 - 195

44
[ 17084-13-8 ]
[ 243982-73-2 ]
[ 141045-26-3 ]
[Ru(2,6-bis(benzimidazol-2-yl)pyridine)(1,3-bis(N-methylbenzimidazol-2-yl)benzene)](PF₆)₂ [ No CAS ]

Yield	Reaction Conditions	Operation in experiment
34.5 mg		To 10 mL dry acetone were added [Ru(H2bip)Cl3] (54 mg,0.10 mmol) and AgOTf (96 mg, 0.37 mmol). The mixture wasrefluxed for 2 h before cooling to room temperature. The resultingAgCl precipitate was removed by filtration, and the filtrate wasconcentrated to dryness. To the residue were added ligand Mebib(36.9 mg, 0.11 mmol), DMF (10 mL), and t-BuOH (10 mL). Themixture was then refluxed for 24 h. After cooling to room temperature,the solventwas removed under reduced pressure, and theresiduewas dissolved in a mixture of 10 mL methanol and 1mL 1Maq. HCl. The mixture was then treated with 100 mg KPF6. Theresulting precipitate was collected by filtration and washing withwater and Et2O. The obtained solid was subjected to flash columnchromatography on silica gel (eluent: CH3CN/H2O/aq.KNO3, 100/10/0.2) to give 34.5 mg of 1(PF6)2 in 37% yield. MALDI-TOF: 749 for [M-2PF6]. Anal. Calcd for C41H30F12N9P2Ru: C, 47.36; H, 2.91; N, 12.12.Found: C, 47.86; H, 3.20; N, 12.09.

Reference： [1]Journal of Organometallic Chemistry,2017,vol. 845,p. 144 - 150

45
[ 17084-13-8 ]
[ 227949-60-2 ]
[ 141045-26-3 ]
terpyridine [ No CAS ]

Reference： [1]Dalton Transactions,2018,vol. 47,p. 9779 - 9786

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H201	Explosive; mass explosion hazard
H202	Explosive; severe projection hazard
H203	Explosive; fire, blast or projection hazard
H204	Fire or projection hazard
H205	May mass explode in fire
H220	Extremely flammable gas
H221	Flammable gas
H222	Extremely flammable aerosol
H223	Flammable aerosol
H224	Extremely flammable liquid and vapour
H225	Highly flammable liquid and vapour
H226	Flammable liquid and vapour
H227	Combustible liquid
H228	Flammable solid
H229	Pressurized container: may burst if heated
H230	May react explosively even in the absence of air
H231	May react explosively even in the absence of air at elevated pressure and/or temperature
H240	Heating may cause an explosion
H241	Heating may cause a fire or explosion
H242	Heating may cause a fire
H250	Catches fire spontaneously if exposed to air
H251	Self-heating; may catch fire
H252	Self-heating in large quantities; may catch fire
H260	In contact with water releases flammable gases which may ignite spontaneously
H261	In contact with water releases flammable gas
H270	May cause or intensify fire; oxidizer
H271	May cause fire or explosion; strong oxidizer
H272	May intensify fire; oxidizer
H280	Contains gas under pressure; may explode if heated
H281	Contains refrigerated gas; may cause cryogenic burns or injury
H290	May be corrosive to metals
Health hazards
Code	Phrase
H300	Fatal if swallowed
H301	Toxic if swallowed
H302	Harmful if swallowed
H303	May be harmful if swallowed
H304	May be fatal if swallowed and enters airways
H305	May be harmful if swallowed and enters airways
H310	Fatal in contact with skin
H311	Toxic in contact with skin
H312	Harmful in contact with skin
H313	May be harmful in contact with skin
H314	Causes severe skin burns and eye damage
H315	Causes skin irritation
H316	Causes mild skin irritation
H317	May cause an allergic skin reaction
H318	Causes serious eye damage
H319	Causes serious eye irritation
H320	Causes eye irritation
H330	Fatal if inhaled
H331	Toxic if inhaled
H332	Harmful if inhaled
H333	May be harmful if inhaled
H334	May cause allergy or asthma symptoms or breathing difficulties if inhaled
H335	May cause respiratory irritation
H336	May cause drowsiness or dizziness
H340	May cause genetic defects
H341	Suspected of causing genetic defects
H350	May cause cancer
H351	Suspected of causing cancer
H360	May damage fertility or the unborn child
H361	Suspected of damaging fertility or the unborn child
H361d	Suspected of damaging the unborn child
H362	May cause harm to breast-fed children
H370	Causes damage to organs
H371	May cause damage to organs
H372	Causes damage to organs through prolonged or repeated exposure
H373	May cause damage to organs through prolonged or repeated exposure
Environmental hazards
Code	Phrase
H400	Very toxic to aquatic life
H401	Toxic to aquatic life
H402	Harmful to aquatic life
H410	Very toxic to aquatic life with long-lasting effects
H411	Toxic to aquatic life with long-lasting effects
H412	Harmful to aquatic life with long-lasting effects
H413	May cause long-lasting harmful effects to aquatic life
H420	Harms public health and the environment by destroying ozone in the upper atmosphere

[ CAS No. 141045-26-3 ] {[proInfo.proName]}

Quality Control of [ 141045-26-3 ]

Related Doc. of [ 141045-26-3 ]

Product Details of [ 141045-26-3 ]

Safety of [ 141045-26-3 ]

Application In Synthesis of [ 141045-26-3 ]

[ 141045-26-3 ] Synthesis Path-Downstream 1~45

Precautionary Statements-General

Prevention

Response

Storage

Disposal

Physical hazards

Health hazards

Environmental hazards

Inquiry