* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Reference:
[1] Journal of the American Chemical Society, 1930, vol. 52, p. 5281
2
[ 110-40-7 ]
[ 2162-98-3 ]
Reference:
[1] Russian Journal of Bioorganic Chemistry, 2002, vol. 28, # 1, p. 62 - 64
3
[ 111-20-6 ]
[ 64-17-5 ]
[ 110-40-7 ]
Reference:
[1] Organic and Biomolecular Chemistry, 2011, vol. 9, # 5, p. 1491 - 1507
[2] Science China Chemistry, 2010, vol. 53, # 12, p. 2452 - 2460
[3] Central European Journal of Chemistry, 2012, vol. 10, # 5, p. 1640 - 1646,7
[4] Journal of Organic Chemistry, 1983, vol. 48, # 18, p. 3106 - 3108
[5] Bulletin de la Societe Chimique de France, 1937, vol. <5> 4, p. 1667
[6] Scientific Papers of the Institute of Physical and Chemical Research (Japan), 1931, vol. 16, p. 15[7] Chem. Zentralbl., 1931, vol. 102, # II, p. 1694
[8] Journal of the Chemical Society, 1948, p. 631
[9] Bl. Inst. phys. chem. Res., 1943, vol. 22, p. 480[10] Chem.Abstr., 1948, p. 1205
[11] Bulletin de la Societe Chimique de France, 1937, vol. <5> 4, p. 1667
[12] Journal of Pharmacy and Pharmacology, 1950, vol. 2, p. 229
[13] Journal of the Chemical Society, 1884, vol. 45, p. 490[14] Journal fuer Praktische Chemie (Leipzig), 1885, vol. <2>32, p. 537
[15] Bulletin de la Societe Chimique de France, 1961, p. 1341 - 1344
[16] Patent: US2013/303796, 2013, A1, . Location in patent: Paragraph 0030; 0034
[17] Green Chemistry, 2016, vol. 18, # 7, p. 2193 - 2200
4
[ 111-20-6 ]
[ 64-17-5 ]
[ 693-55-0 ]
[ 110-40-7 ]
Reference:
[1] Langmuir, 2012, vol. 28, # 11, p. 4955 - 4964
[2] Journal of the Chemical Society, 1876, vol. 29, p. 315[3] Jahresbericht ueber die Fortschritte der Chemie und Verwandter Theile Anderer Wissenschaften, 1876, p. 576
5
[ 64-17-5 ]
[ 692-86-4 ]
[ 110-40-7 ]
Reference:
[1] Canadian Journal of Chemistry, 1962, vol. 40, p. 1189 - 1195
[2] Canadian Journal of Chemistry, 1965, vol. 43, p. 319 - 327
6
[ 626-86-8 ]
[ 110-40-7 ]
Reference:
[1] Helvetica Chimica Acta, 1935, vol. 18, p. 449
[2] Kanazawa Daigaku Yakugakubu Kenkyu Nempo, 1952, vol. 2, p. 30,35[3] Chem.Abstr., 1955, p. 1565
[4] Aromatics Japan, 1949, # 8, p. 18,20[5] Chem.Abstr., 1950, p. 5828
7
[ 693-55-0 ]
[ 111-20-6 ]
[ 110-40-7 ]
Reference:
[1] Chemische Berichte, 1922, vol. 55, p. 2218
8
[ 42367-85-1 ]
[ 539-82-2 ]
[ 1968-40-7 ]
[ 141-28-6 ]
[ 110-40-7 ]
Reference:
[1] Helvetica Chimica Acta, 1935, vol. 18, p. 449
With acidic cation exchange resin Amberlyst 70; at 50 - 160℃;Flow reactor; Green chemistry;
General procedure: Decanedioic acid and various alcohols at a respective weight ratio of 1:5 were mixed respectively at 50 C., and introduced into the lower part of the vertical reactor at a liquid hourly space velocity (LHSV) of 6 hour-1. The reaction temperature was 160 C. The analysis results of the products were shown in Table 2.
(1) 40.5 g of sebacic acid and 25.8 g of <strong>[110-40-7]diethyl sebacate</strong> were stirred at 100 C. in di n-butylether in the presence of conc. hydrochloric acid for 5 hours while ethanol was added dropwise. Subsequently, the mixture was poured into hexane, then the precipitated sebacic acid was removed, and subjected to extraction with aqueous alkali solution. The resulting extract was acidified, and extracted with ethyl acetate, and further concentrated, to obtain 9-ethoxycarbonylnonanoic acid in an amount of 23.4 g in a yield of 50.8%.